[C₆H₅PHC(CH₃)2C₅H₄]2Fe

Base Information

• Chemical Name: [C₆H₅PHC(CH₃)2C₅H₄]2Fe
• CAS No.: 446062-43-7
• Molecular Formula: C₂₈H₃₂FeP₂
• Molecular Weight: 486.357

Synonyms:

Chemical Property of [C₆H₅PHC(CH₃)2C₅H₄]2Fe

Chemical Property:

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Technology Process of [C₆H₅PHC(CH₃)2C₅H₄]2Fe

There total 1 articles about [C₆H₅PHC(CH₃)2C₅H₄]2Fe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

Li(1+)*C5H4C(CH3)2PH(C6H5)(1-)=Li[C5H4C(CH3)2PH(C6H5)] + iron(II) chloride → [C6H5PHC(CH3)2C5H4]2Fe (446062-43-7)

Guidance literature:

In tetrahydrofuran; byproducts: LiCl; under dry Ar, 2 equiv. of Li-compd. was added in THF to THF suspn. of FeCl2, stirring for 16 h at room temp.; solvent was removed in vac., Et2O was added, soln. was filtered, residuewas extd. repeatedly with Et2O, solvent was removed from combined Et2O fraction in vac., residue was recrystd. repeatedly from n-pentane (or n- hexane) at -20 °C, elem. anal.;

DOI:10.1002/1099-0682(200205)2002:5<1174::AID-EJIC1174>3.0.CO;2-A

Reference yield: 45.0%

pentamethylcyclopentadienyl tantalum(V) tetrachloride + [C6H5PHC(CH3)2C5H4]2Fe (446062-43-7) → [(C5(CH3)5TaCl4)C6H5PHC(CH3)2C5H4]2Fe

Guidance literature:

In toluene; under dry Ar, 0.5 equiv. of Fe-compd. was added in toluene to toluene suspn. of Ta-compd., heating at 70 °C for 2 h, mixt. was allowed tocool, stirring at room temp. overnight; soln. was filtered, cooled to -20 °C, excess of Ta-compd. was sepd., soln. was evapd. in vac., residue was extd. with CH2Cl2, soln. was concd., cooled to -20 °C, solid was recrystd. repeatedly from toluene;

DOI:10.1002/1099-0682(200205)2002:5<1174::AID-EJIC1174>3.0.CO;2-A

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