3-methoxy-6-[(4-methoxybenzyl)oxy]-5,7-dimethyl-1-octen-4-ol

Base Information

Chemical Name:3-methoxy-6-[(4-methoxybenzyl)oxy]-5,7-dimethyl-1-octen-4-ol
CAS No.:443283-18-9
Molecular Formula:C₁₉H₃₀O₄
Molecular Weight:322.445
Hs Code.:

Synonyms:

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Chemical Property of 3-methoxy-6-[(4-methoxybenzyl)oxy]-5,7-dimethyl-1-octen-4-ol

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Technology Process of 3-methoxy-6-[(4-methoxybenzyl)oxy]-5,7-dimethyl-1-octen-4-ol

There total 6 articles about 3-methoxy-6-[(4-methoxybenzyl)oxy]-5,7-dimethyl-1-octen-4-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108735-30-4
[3R,4S,4'S]-4-[acyl(4'-isopropyl-2'-oxazolidone)]-2-methylhex-5-en-3-ol

: 443283-18-9
3-methoxy-6-[(4-methoxybenzyl)oxy]-5,7-dimethyl-1-octen-4-ol

Guidance literature:: Multi-step reaction with 7 steps

1.1: tributylborane; acetic acid / tetrahydrofuran / 1.5 h / 23 °C

1.2: lithium borohydride / tetrahydrofuran / 1 h / 0 °C

1.3: 85 percent / H₂O₂ / tetrahydrofuran; H₂O / 1 h / 0 °C / pH 7

2.1: 81 percent / pyridine / 4 h / 23 °C

3.1: 66 percent / lithium aluminum hydride / diethyl ether / -25 °C

4.1: sodium hydride / dimethylsulfoxide; tetrahydrofuran / 0.5 h / 23 °C

4.2: 86 percent / tetrahydrofuran; dimethylsulfoxide / 23 °C

5.1: N-methylmorpholine N-oxide / osmium tetroxide / acetone; tetrahydrofuran; H₂O / 3 h / 23 °C / pH 7.0

6.1: aq. NaIO₄ / tetrahydrofuran; H₂O / 23 °C / pH 7.0

7.1: 60 mg / chromium(II) chloride; trimethylsilyl iodide / 4.5 h / -42 °C

With pyridine; chromium dichloride; sodium periodate; lithium aluminium tetrahydride; trimethylsilyl iodide; tributyl borane; sodium hydride; acetic acid; 4-methylmorpholine N-oxide; osmium(VIII) oxide; In tetrahydrofuran; diethyl ether; water; dimethyl sulfoxide; acetone; 7.1: Takai reaction;
DOI:10.1021/jo016413f

Reference yield:

: 443283-04-3
[3R,4R]-3-hydroxymethyl-5-methylhex-1-en-4-ol

: 443283-18-9
3-methoxy-6-[(4-methoxybenzyl)oxy]-5,7-dimethyl-1-octen-4-ol

Guidance literature:: Multi-step reaction with 6 steps

1.1: 81 percent / pyridine / 4 h / 23 °C

2.1: 66 percent / lithium aluminum hydride / diethyl ether / -25 °C

3.1: sodium hydride / dimethylsulfoxide; tetrahydrofuran / 0.5 h / 23 °C

3.2: 86 percent / tetrahydrofuran; dimethylsulfoxide / 23 °C

4.1: N-methylmorpholine N-oxide / osmium tetroxide / acetone; tetrahydrofuran; H₂O / 3 h / 23 °C / pH 7.0

5.1: aq. NaIO₄ / tetrahydrofuran; H₂O / 23 °C / pH 7.0

6.1: 60 mg / chromium(II) chloride; trimethylsilyl iodide / 4.5 h / -42 °C

With pyridine; chromium dichloride; sodium periodate; lithium aluminium tetrahydride; trimethylsilyl iodide; sodium hydride; 4-methylmorpholine N-oxide; osmium(VIII) oxide; In tetrahydrofuran; diethyl ether; water; dimethyl sulfoxide; acetone; 6.1: Takai reaction;
DOI:10.1021/jo016413f

Reference yield:

: 443283-05-4
[3S,4R]-3,5-dimethyl-4-[(4-methoxybenzyl)oxy]hex-1-ene

: 443283-18-9
3-methoxy-6-[(4-methoxybenzyl)oxy]-5,7-dimethyl-1-octen-4-ol

Guidance literature:: Multi-step reaction with 3 steps

1: N-methylmorpholine N-oxide / osmium tetroxide / acetone; tetrahydrofuran; H₂O / 3 h / 23 °C / pH 7.0

2: aq. NaIO₄ / tetrahydrofuran; H₂O / 23 °C / pH 7.0

3: 60 mg / chromium(II) chloride; trimethylsilyl iodide / 4.5 h / -42 °C

With chromium dichloride; sodium periodate; trimethylsilyl iodide; 4-methylmorpholine N-oxide; osmium(VIII) oxide; In tetrahydrofuran; water; acetone; 3: Takai reaction;
DOI:10.1021/jo016413f