1-(phenylsulfonyl)indole-2,3-dicarboxylic N-benzylimide

Base Information

Chemical Name:1-(phenylsulfonyl)indole-2,3-dicarboxylic N-benzylimide
CAS No.:1527486-06-1
Molecular Formula:C₂₃H₁₆N₂O₄S
Molecular Weight:416.457
Hs Code.:

Synonyms:

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Chemical Property of 1-(phenylsulfonyl)indole-2,3-dicarboxylic N-benzylimide

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Technology Process of 1-(phenylsulfonyl)indole-2,3-dicarboxylic N-benzylimide

There total 6 articles about 1-(phenylsulfonyl)indole-2,3-dicarboxylic N-benzylimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1527486-05-0
2-benzyl-2,4-dihydro-3-n-pentyl-4-(phenylsulfonyl)pyrrolo[3,4-b]indole

: 1527486-06-1
1-(phenylsulfonyl)indole-2,3-dicarboxylic N-benzylimide

Guidance literature:: With air; In hexane; ethyl acetate; Reflux;

Reference yield:

: 83-34-1
3-Methylindole

: 1527486-06-1
1-(phenylsulfonyl)indole-2,3-dicarboxylic N-benzylimide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate / dichloromethane / 4 h / 0 - 20 °C

2.1: sec.-butyllithium / tetrahydrofuran; cyclohexane / 3 h / -70 - 20 °C

2.2: -70 °C

3.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 8 h / Reflux

4.1: chloroform / 24 h / 20 °C / Inert atmosphere

5.1: air / ethyl acetate; hexane / Reflux

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sec.-butyllithium; tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In tetrahydrofuran; tetrachloromethane; hexane; dichloromethane; chloroform; cyclohexane; ethyl acetate;

Reference yield:

: 58550-84-8
N-(phenylsulphonyl)-3-methylindole

: 1527486-06-1
1-(phenylsulfonyl)indole-2,3-dicarboxylic N-benzylimide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sec.-butyllithium / tetrahydrofuran; cyclohexane / 3 h / -70 - 20 °C

1.2: -70 °C

2.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 8 h / Reflux

3.1: chloroform / 24 h / 20 °C / Inert atmosphere

4.1: air / ethyl acetate; hexane / Reflux

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); sec.-butyllithium; In tetrahydrofuran; tetrachloromethane; hexane; chloroform; cyclohexane; ethyl acetate;