C₄₂H₆₂N₆O₁₀S

Base Information

Chemical Name:C₄₂H₆₂N₆O₁₀S
CAS No.:1647153-72-7
Molecular Formula:C₄₂H₆₂N₆O₁₀S
Molecular Weight:843.054
Hs Code.:

C<sub>42</sub>H<sub>62</sub>N<sub>6</sub>O<sub>10</sub>S

Synonyms:

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Chemical Property of C₄₂H₆₂N₆O₁₀S

Chemical Property:

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Technology Process of C₄₂H₆₂N₆O₁₀S

There total 8 articles about C₄₂H₆₂N₆O₁₀S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1647153-47-6
(2R,3S)-2-(tert-butyloxycarbonylamino)-1-O-(tert-butyldimethylsilyl)-4-methyl-pentane-1,3-diol

: 1647153-72-7
C₄₂H₆₂N₆O₁₀S

Guidance literature:: Multi-step reaction with 5 steps

1: boron trifluoride diethyl etherate / acetone / 23 h / 20 °C

2: ruthenium trichloride; sodium periodate / water; tetrachloromethane; acetonitrile / 4 h / 0 °C

3: caesium carbonate / N,N-dimethyl-formamide / 20 h / 20 °C / Inert atmosphere

4: dichloromethane / 19 h / 20 °C

5: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide; tert-butyl alcohol / 23 h / 20 °C / Inert atmosphere

With ruthenium trichloride; sodium periodate; boron trifluoride diethyl etherate; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; caesium carbonate; N-ethyl-N,N-diisopropylamine; In tetrachloromethane; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; tert-butyl alcohol;
DOI:10.3762/bjoc.10.113

Reference yield:

: 188802-09-7
(2R,3S)-1-(tert-Butyl-dimethyl-silanyloxy)-2-dibenzylamino-4-methyl-pentan-3-ol

: 1647153-72-7
C₄₂H₆₂N₆O₁₀S

Guidance literature:: Multi-step reaction with 7 steps

1: 10 wt% Pd(OH)2 on carbon; hydrogen / methanol

2: sodium hydrogencarbonate / tetrahydrofuran; water / 19 h / 0 - 20 °C

3: boron trifluoride diethyl etherate / acetone / 23 h / 20 °C

4: ruthenium trichloride; sodium periodate / water; tetrachloromethane; acetonitrile / 4 h / 0 °C

5: caesium carbonate / N,N-dimethyl-formamide / 20 h / 20 °C / Inert atmosphere

6: dichloromethane / 19 h / 20 °C

7: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide; tert-butyl alcohol / 23 h / 20 °C / Inert atmosphere

With ruthenium trichloride; sodium periodate; 10 wt% Pd(OH)2 on carbon; boron trifluoride diethyl etherate; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; sodium hydrogencarbonate; caesium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; tetrachloromethane; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; tert-butyl alcohol;
DOI:10.3762/bjoc.10.113

Reference yield:

: 188802-11-1
(2R,3S)-2-Amino-1-(tert-butyl-dimethyl-silanyloxy)-4-methyl-pentan-3-ol

: 1647153-72-7
C₄₂H₆₂N₆O₁₀S

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydrogencarbonate / tetrahydrofuran; water / 19 h / 0 - 20 °C

2: boron trifluoride diethyl etherate / acetone / 23 h / 20 °C

3: ruthenium trichloride; sodium periodate / water; tetrachloromethane; acetonitrile / 4 h / 0 °C

4: caesium carbonate / N,N-dimethyl-formamide / 20 h / 20 °C / Inert atmosphere

5: dichloromethane / 19 h / 20 °C

6: N-ethyl-N,N-diisopropylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide; tert-butyl alcohol / 23 h / 20 °C / Inert atmosphere

With ruthenium trichloride; sodium periodate; boron trifluoride diethyl etherate; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; sodium hydrogencarbonate; caesium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; tetrachloromethane; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile; tert-butyl alcohol;
DOI:10.3762/bjoc.10.113