trans-6-<5-(4-acetoxycyclohexyl)pentyl>-2,3-dimethoxy-5-methyl-1,4-benzoquinone

Base Information

Chemical Name:trans-6-<5-(4-acetoxycyclohexyl)pentyl>-2,3-dimethoxy-5-methyl-1,4-benzoquinone
CAS No.:107228-74-0
Molecular Formula:C₂₂H₃₂O₆
Molecular Weight:392.492
Hs Code.:

Synonyms:

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Chemical Property of trans-6-<5-(4-acetoxycyclohexyl)pentyl>-2,3-dimethoxy-5-methyl-1,4-benzoquinone

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Technology Process of trans-6-<5-(4-acetoxycyclohexyl)pentyl>-2,3-dimethoxy-5-methyl-1,4-benzoquinone

There total 6 articles about trans-6-<5-(4-acetoxycyclohexyl)pentyl>-2,3-dimethoxy-5-methyl-1,4-benzoquinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107228-87-5
6-(4-methoxyphenyl)-hexan-1-oic acid

: 107228-74-0
trans-6-<5-(4-acetoxycyclohexyl)pentyl>-2,3-dimethoxy-5-methyl-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 6 steps

1: 48 percent HBr / acetic acid

2: 11.5 percent / hydrogen / 5 percent Rh-C / ethanol / 1.17 h / 7428.6 Torr / Ambient temperature

3: 82.4 percent / p-TsOH / 1 h / 60 - 70 °C

4: SOCl₂ / Ambient temperature

5: Na₂O₂ / petroleum ether; H₂O / 0 °C

6: 0.814 g / acetic acid / 1 h / 120 °C

With thionyl chloride; sodium peroxide; hydrogen bromide; hydrogen; toluene-4-sulfonic acid; Rh on carbon; In ethanol; water; acetic acid; Petroleum ether;
DOI:10.1248/cpb.36.178

Reference yield:

: 6952-35-8
6-(4-hydroxyphenyl)hexanoic acid

: 107228-74-0
trans-6-<5-(4-acetoxycyclohexyl)pentyl>-2,3-dimethoxy-5-methyl-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 5 steps

1: 11.5 percent / hydrogen / 5 percent Rh-C / ethanol / 1.17 h / 7428.6 Torr / Ambient temperature

2: 82.4 percent / p-TsOH / 1 h / 60 - 70 °C

3: SOCl₂ / Ambient temperature

4: Na₂O₂ / petroleum ether; H₂O / 0 °C

5: 0.814 g / acetic acid / 1 h / 120 °C

With thionyl chloride; sodium peroxide; hydrogen; toluene-4-sulfonic acid; Rh on carbon; In ethanol; water; acetic acid; Petroleum ether;
DOI:10.1248/cpb.36.178

Reference yield:

: 5537-76-8
6-(4-methoxyphenyl)-6-oxohexanoic acid

: 107228-74-0
trans-6-<5-(4-acetoxycyclohexyl)pentyl>-2,3-dimethoxy-5-methyl-1,4-benzoquinone

Guidance literature:: Multi-step reaction with 7 steps

1: Clemmensen reduction

2: 48 percent HBr / acetic acid

3: 11.5 percent / hydrogen / 5 percent Rh-C / ethanol / 1.17 h / 7428.6 Torr / Ambient temperature

4: 82.4 percent / p-TsOH / 1 h / 60 - 70 °C

5: SOCl₂ / Ambient temperature

6: Na₂O₂ / petroleum ether; H₂O / 0 °C

7: 0.814 g / acetic acid / 1 h / 120 °C

With thionyl chloride; sodium peroxide; hydrogen bromide; hydrogen; toluene-4-sulfonic acid; Rh on carbon; In ethanol; water; acetic acid; Petroleum ether;
DOI:10.1248/cpb.36.178