C₇₁H₁₂₀O₁₃Si₃

Base Information

Chemical Name:C₇₁H₁₂₀O₁₃Si₃
CAS No.:902454-77-7
Molecular Formula:C₇₁H₁₂₀O₁₃Si₃
Molecular Weight:1265.98
Hs Code.:

C<sub>71</sub>H<sub>120</sub>O<sub>13</sub>Si<sub>3</sub>

Synonyms:

Suppliers and Price of C₇₁H₁₂₀O₁₃Si₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₇₁H₁₂₀O₁₃Si₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₇₁H₁₂₀O₁₃Si₃

There total 32 articles about C₇₁H₁₂₀O₁₃Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₇₇H₁₃₂N₂O₁₃Si₃

: 902454-77-7
C₇₁H₁₂₀O₁₃Si₃

Guidance literature:: With oxalic acid; In diethyl ether; at 25 ℃; for 48h;
DOI:10.1039/b602021f

Reference yield:

: 902454-48-2
C₁₀H₂₀O₃

: 902454-77-7
C₇₁H₁₂₀O₁₃Si₃

Guidance literature:: Multi-step reaction with 18 steps

1.1: NaH / tetrahydrofuran; various solvent(s) / 0.5 h / 0 °C

2.1: O₃ / CH₂Cl₂ / -78 °C

2.2: PPh₃ / CH₂Cl₂ / 1 h / -78 - 25 °C

3.1: 28.9 g / benzene / 40 h / 70 °C

4.1: 96 percent / DIBAL-H / toluene; tetrahydrofuran / 2.5 h / -78 °C

5.1: TsOH*H₂O / acetone / 3 h / 25 °C

6.1: 25.84 g / imidazole; 4-DMAP / CH₂Cl₂ / 1.5 h / 25 °C

7.1: 78 percent / NaH₂PO₄; NaClO₂; 2-methyl-2-butene / 2-methyl-propan-2-ol; H₂O / 2 h / 25 °C

8.1: 97 percent / K₂CO₃ / acetone / 16 h / 25 °C

9.1: KHMDS / tetrahydrofuran; toluene / 0.5 h / -78 °C

9.2: Davis oxaziridine / tetrahydrofuran; toluene / 1 h / -78 °C

10.1: 86 percent / imidazole; 4-DMAP / CH₂Cl₂ / 16 h / 25 °C

11.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

11.2: 92 percent / tetrahydrofuran; hexane / 1 h / -78 °C

12.1: LiCl / acetonitrile / 0.17 h / 25 °C

12.2: i-Pr₂NEt / acetonitrile / 0.17 h / 25 °C

12.3: 97 percent / acetonitrile / 36 h / 25 °C

13.1: KHMDS / tetrahydrofuran; toluene / 0.5 h / 25 °C

13.2: 94 percent / tetrahydrofuran; toluene / -78 - 25 °C

14.1: 87 percent / PPTS / ethanol / 20 h / 45 °C

15.1: Et₃N / tetrahydrofuran / 1 h / 0 - 25 °C

16.1: 1.04 g / LiBr / tetrahydrofuran / 0.5 h / 25 °C

17.1: LDA / tetrahydrofuran / 1 h / -78 °C

17.2: tetrahydrofuran / 1 h / -78 °C

18.1: 0.710 g / aq. (CO₂H)2 / diethyl ether / 48 h / 25 °C

With 1H-imidazole; dmap; sodium chlorite; sodium dihydrogenphosphate; n-butyllithium; 2-methyl-but-2-ene; pyridinium p-toluenesulfonate; oxalic acid; potassium hexamethylsilazane; sodium hydride; diisobutylaluminium hydride; potassium carbonate; toluene-4-sulfonic acid; ozone; triethylamine; lithium chloride; lithium bromide; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; ethanol; hexane; dichloromethane; water; acetone; toluene; acetonitrile; tert-butyl alcohol; benzene; 3.1: Wittig reaction / 12.1: Horner-Wadsworth-Emmons olefination / 13.2: Wittig methylenation;
DOI:10.1039/b602021f

Reference yield:

: 902132-32-5
C₁₃H₂₆O₃Si

: 902454-77-7
C₇₁H₁₂₀O₁₃Si₃

Guidance literature:: Multi-step reaction with 8 steps

1.1: O₃ / CH₂Cl₂ / -78 °C

1.2: 88 percent / PPh₃ / CH₂Cl₂ / 1 h / -78 - 25 °C

2.1: LiCl / acetonitrile / 0.17 h / 25 °C

2.2: i-Pr₂NEt / acetonitrile / 0.17 h / 25 °C

2.3: acetonitrile / 48 h / 25 °C

3.1: KHMDS / tetrahydrofuran; toluene / 0.5 h / 25 °C

3.2: 94 percent / tetrahydrofuran; toluene / -78 - 25 °C

4.1: 87 percent / PPTS / ethanol / 20 h / 45 °C

5.1: Et₃N / tetrahydrofuran / 1 h / 0 - 25 °C

6.1: 1.04 g / LiBr / tetrahydrofuran / 0.5 h / 25 °C

7.1: LDA / tetrahydrofuran / 1 h / -78 °C

7.2: tetrahydrofuran / 1 h / -78 °C

8.1: 0.710 g / aq. (CO₂H)2 / diethyl ether / 48 h / 25 °C

With pyridinium p-toluenesulfonate; oxalic acid; potassium hexamethylsilazane; ozone; triethylamine; lithium chloride; lithium bromide; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; toluene; acetonitrile; 2.1: Horner-Wadsworth-Emmons olefination / 3.2: Wittig methylenation;
DOI:10.1039/b602021f