potassium fac-trihydrido tris(dimethylphenylphosphino)osmate

Base Information

• Chemical Name: potassium fac-trihydrido tris(dimethylphenylphosphino)osmate
• CAS No.: 93895-80-8
• Molecular Formula: C₂₄H₃₆OsP₃*K
• Molecular Weight: 646.769

Synonyms:

Chemical Property of potassium fac-trihydrido tris(dimethylphenylphosphino)osmate

Chemical Property:

Purity/Quality:

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Technology Process of potassium fac-trihydrido tris(dimethylphenylphosphino)osmate

There total 2 articles about potassium fac-trihydrido tris(dimethylphenylphosphino)osmate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

OsH4(P(CH3)2C6H5)3 (24228-57-7,64912-35-2) + potassium hydride → potassium fac-trihydrido tris(dimethylphenylphosphino)osmate (106061-75-0,93895-80-8)

Guidance literature:

In tetrahydrofuran; byproducts: H2; heating at 70°C for 12 h; NMR monitoring; filtration;

DOI:10.1021/ja00304a016

Reference yield:

OsH4(P(CH3)2C6H5)3 (24228-57-7,64912-35-2) + potassium hydride → potassium fac-trihydrido tris(dimethylphenylphosphino)osmate (106061-75-0,93895-80-8)

Guidance literature:

In tetrahydrofuran; excess of KH, 70°C, 12 h; filtration;

Reference yield:

potassium fac-trihydrido tris(dimethylphenylphosphino)osmate (106061-75-0,93895-80-8) → OsH4(P(CH3)2C6H5)3 (24228-57-7,64912-35-2)

Guidance literature:

With H₂O; In tetrahydrofuran; NMR monitoring;

DOI:10.1021/ja00304a016

upstream raw materials:

OsH₄(P(CH₃)2C₆H₅)3

OsH₄(P(CH₃)2C₆H₅)3

Downstream raw materials:

OsH₄(P(CH₃)2C₆H₅)3

OsH₄(P(CH₃)2C₆H₅)3

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