C₂₃H₃₀N₂O₂

Base Information

• Chemical Name: C₂₃H₃₀N₂O₂
• CAS No.: 1243251-67-3
• Molecular Formula: C₂₃H₃₀N₂O₂
• Molecular Weight: 366.503
• Mol file: 1243251-67-3.mol

Synonyms:

Chemical Property of C₂₃H₃₀N₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₃H₃₀N₂O₂

There total 4 articles about C₂₃H₃₀N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-methyl-butan-2-one (563-80-4) → C23H30N2O2 (1243251-67-3)

Guidance literature:

Multi-step reaction with 4 steps

1.1: ethanol; sodium / 4 h / 10 °C

2.1: sodium hydrogencarbonate / methanol / 2 h / 0 - 60 °C

2.2: 2 h / 80 °C

2.3: pH 3

3.1: thionyl chloride / 8 h / Reflux

4.1: pyridine / acetonitrile / 8 h / Reflux

With pyridine; thionyl chloride; ethanol; sodium; sodium hydrogencarbonate; In methanol; acetonitrile; 1.1: Claisen condensation;

DOI:10.1021/jf104712c

Reference yield:

2-phenyl-5-isopropyl-2H-pyrazole-3-carboxylic acid (299165-57-4) → C23H30N2O2 (1243251-67-3)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride / 8 h / Reflux

2: pyridine / acetonitrile / 8 h / Reflux

With pyridine; thionyl chloride; In acetonitrile;

DOI:10.1021/jf104712c

Reference yield:

ethyl 2,4-dioxo-5-methylhexanoate (64195-85-3) → C23H30N2O2 (1243251-67-3)

Guidance literature:

Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate / methanol / 2 h / 0 - 60 °C

1.2: 2 h / 80 °C

1.3: pH 3

2.1: thionyl chloride / 8 h / Reflux

3.1: pyridine / acetonitrile / 8 h / Reflux

With pyridine; thionyl chloride; sodium hydrogencarbonate; In methanol; acetonitrile;

DOI:10.1021/jf104712c

upstream raw materials:

3-methyl-butan-2-one

Geraniol

3-isopropyl-1-phenyl-pyrazol-5-carbonyl chloride

2-phenyl-5-isopropyl-2H-pyrazole-3-carboxylic acid