3-bromo 2,4,5,6-tetrafluoro phenyllithium

Base Information

Chemical Name:3-bromo 2,4,5,6-tetrafluoro phenyllithium
CAS No.:199588-22-2
Molecular Formula:C₆BrF₄Li
Molecular Weight:234.905
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-bromo 2,4,5,6-tetrafluoro phenyllithium

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Technology Process of 3-bromo 2,4,5,6-tetrafluoro phenyllithium

There total 1 articles about 3-bromo 2,4,5,6-tetrafluoro phenyllithium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 109-72-8,29786-93-4
n-butyllithium

: 1559-87-1
1,3-dibromo-2,4,5,6-tetrafluorobenzene

: 199588-22-2
3-bromo 2,4,5,6-tetrafluoro phenyllithium

Guidance literature:: In diethyl ether; equimolar amounts of 1,3-Br2C6F4 and n-C4H9Li;;

Reference yield: 71.0%

: 12107-56-1
dichloro(cycloocta-1,5-diene)palladium (II)

: 199588-22-2
3-bromo 2,4,5,6-tetrafluoro phenyllithium

: 199588-29-9
cis-[Pd(COD)(m-bromotetrafluorophenyl)2]

Guidance literature:: In diethyl ether; byproducts: LiCl; N2-atmosphere; mixing at -78°C, warming; addn. of H2O, evapn., extn. (CH2Cl2), concn., addn. of EtOH, crystn. on standing at -28°C, collection (filtration), washing (EtOH), drying; elem. anal.;
DOI:10.1021/om970529d