Technology Process of C19H21NO3
There total 1 articles about C19H21NO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
tetrahydrofuran; diethyl ether;
at 0 ℃;
for 0.0666667h;
Inert atmosphere;
DOI:10.1002/anie.201104487
- Guidance literature:
-
With
sodium tetrahydroborate; acetic acid;
In
methanol;
at 0 - 20 ℃;
chemoselective reaction;
Inert atmosphere;
DOI:10.1002/anie.201104487
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium tetrahydroborate; acetic acid / methanol / 0 - 20 °C / Inert atmosphere
2.1: trifluorormethanesulfonic acid / dichloromethane / 0.08 h / 0 °C / Inert atmosphere
3.1: tert.-butylhydroperoxide; N-benzyl-trimethylammonium hydroxide / tetrahydrofuran; methanol; water / 17 h / 23 °C / Inert atmosphere
3.2: 2 h / Inert atmosphere
With
tert.-butylhydroperoxide; sodium tetrahydroborate; trifluorormethanesulfonic acid; N-benzyl-trimethylammonium hydroxide; acetic acid;
In
tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/anie.201104487