cis-[(PMePh₂)2Pt(N-(9-methyl-1,9-dihydro-purin-6-ylidene)-acetamidine(-1H))]NO₃

Base Information

Chemical Name:cis-[(PMePh₂)2Pt(N-(9-methyl-1,9-dihydro-purin-6-ylidene)-acetamidine(-1H))]NO₃
CAS No.:880000-65-7
Molecular Formula:C₃₄H₃₅N₆P₂Pt*NO₃
Molecular Weight:846.725
Hs Code.:

cis-[(PMePh<sub>2</sub>)2Pt(N-(9-methyl-1,9-dihydro-purin-6-ylidene)-acetamidine(-1H))]NO<sub>3</sub>

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Chemical Property of cis-[(PMePh₂)2Pt(N-(9-methyl-1,9-dihydro-purin-6-ylidene)-acetamidine(-1H))]NO₃

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Technology Process of cis-[(PMePh₂)2Pt(N-(9-methyl-1,9-dihydro-purin-6-ylidene)-acetamidine(-1H))]NO₃

There total 1 articles about cis-[(PMePh₂)2Pt(N-(9-methyl-1,9-dihydro-purin-6-ylidene)-acetamidine(-1H))]NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 700-00-5
3-methyladenine

: di(cis-[bis(methyldiphenylphosphane)(μ-hydroxo)platinum(II)]) nitrate

: 75-05-8,26809-02-9
acetonitrile

: 880000-65-7
cis-[(PMePh₂)2Pt(N-(9-methyl-1,9-dihydro-purin-6-ylidene)-acetamidine(-1H))]NO₃

Guidance literature:: In acetonitrile; byproducts: Pt, H2O; stirred for ca 1 h, heated at 50°C for 12 h; filtered, crystd. at room temp. for 2-3 d, sepd., dried (vac.); the remaining soln. pptd. (Et2O), filtered, washed (Et2O), dried (vac.); the recovered solid dissolved in MeCN, pptd. (Et2O); elem. anal.;
DOI:10.1021/ic051755f

Reference yield:

: 880000-65-7
cis-[(PMePh₂)2Pt(N-(9-methyl-1,9-dihydro-purin-6-ylidene)-acetamidine(-1H))]NO₃

: cis-[(PPh₂Me)Pt(9-methyladenine(-1H))]3(NO₃)3

Guidance literature:: In chloroform; byproducts: CH3CN; equil. at room temp. in soln.; not isolated, detected by NMR;
DOI:10.1021/ic051755f

Reference yield:

: 31432-55-0
1-[13C]acetonitrile

: 880000-65-7
cis-[(PMePh₂)2Pt(N-(9-methyl-1,9-dihydro-purin-6-ylidene)-acetamidine(-1H))]NO₃

: cis-[(PMePh₂)2Pt(N-(9-methyl-1,9-dihydro-purin-6-ylidene)-acetamidine(-1H))]NO₃

Guidance literature:: In further solvent(s); for hours at room temp. in a mixt. of CD3CN and CH3(13)CN; not isolated, detected by NMR;
DOI:10.1021/ic051755f