Technology Process of C26H32N2O4
There total 8 articles about C26H32N2O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C27H28N2O5;
With
borane dimethyl sulphide complex;
In
tetrahydrofuran;
at 0 - 60 ℃;
With
methanol;
DOI:10.1016/j.bmcl.2011.11.072
- Guidance literature:
-
Multi-step reaction with 6 steps
1: potassium carbonate / N,N-dimethyl-formamide
2: sodium tetrahydroborate / methanol
3: sodium hydrogencarbonate / N,N-dimethyl-formamide
4: lithium aluminium tetrahydride / tetrahydrofuran
5: toluene / 1 h / 20 °C
6: borane dimethyl sulphide complex / tetrahydrofuran / 0 - 60 °C
With
sodium tetrahydroborate; lithium aluminium tetrahydride; borane dimethyl sulphide complex; sodium hydrogencarbonate; potassium carbonate;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2011.11.072
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydrogencarbonate / N,N-dimethyl-formamide
2: lithium aluminium tetrahydride / tetrahydrofuran
3: toluene / 1 h / 20 °C
4: borane dimethyl sulphide complex / tetrahydrofuran / 0 - 60 °C
With
lithium aluminium tetrahydride; borane dimethyl sulphide complex; sodium hydrogencarbonate;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1016/j.bmcl.2011.11.072