C₂₃H₃₂O₆

Base Information

Chemical Name:C₂₃H₃₂O₆
CAS No.:1384271-82-2
Molecular Formula:C₂₃H₃₂O₆
Molecular Weight:404.503
Hs Code.:

C<sub>23</sub>H<sub>32</sub>O<sub>6</sub>

Synonyms:

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Chemical Property of C₂₃H₃₂O₆

Chemical Property:

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Technology Process of C₂₃H₃₂O₆

There total 14 articles about C₂₃H₃₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1384271-73-1
C₁₃H₂₂O₃

: 1384271-82-2
C₂₃H₃₂O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: 1H-imidazole / dichloromethane / 0 - 20 °C

2.1: methanol; toluene-4-sulfonic acid / 0 - 20 °C

3.1: sodium tetrahydroborate; nickel diacetate / ethanol; ethylene glycol / 6 h / 20 °C

4.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / dichloromethane / 12 h / -20 °C / Molecular sieve

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C

5.2: -78 °C

6.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 - 20 °C

7.1: scandium tris(trifluoromethanesulfonate) / tetrahydrofuran; water / 12 h / 20 °C

8.1: camphor-10-sulfonic acid / dichloromethane / 0 - 20 °C

9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

10.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 4 h / 0 - 20 °C

10.2: 12 h / 0 - 20 °C

11.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / Reflux

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; titanium(IV) isopropylate; methanol; tert.-butylhydroperoxide; sodium tetrahydroborate; oxalyl dichloride; L-(+)-diisopropyl tartrate; 2,4,6-trichlorobenzoyl chloride; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; nickel diacetate; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; ethanol; dichloromethane; water; ethylene glycol; 4.1: Sharpless epoxidation / 5.1: Swern oxidation / 5.2: Swern oxidation / 10.1: Yamaguchi reaction / 10.2: Yamaguchi reaction;
DOI:10.1016/j.tetlet.2012.04.118

Reference yield:

: 1384271-75-3
C₂₉H₄₀O₃Si

: 1384271-82-2
C₂₃H₃₂O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: methanol; toluene-4-sulfonic acid / 0 - 20 °C

2.1: sodium tetrahydroborate; nickel diacetate / ethanol; ethylene glycol / 6 h / 20 °C

3.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; L-(+)-diisopropyl tartrate / dichloromethane / 12 h / -20 °C / Molecular sieve

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / -78 °C

4.2: -78 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 - 20 °C

6.1: scandium tris(trifluoromethanesulfonate) / tetrahydrofuran; water / 12 h / 20 °C

7.1: camphor-10-sulfonic acid / dichloromethane / 0 - 20 °C

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

9.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 4 h / 0 - 20 °C

9.2: 12 h / 0 - 20 °C

10.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / Reflux

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; titanium(IV) isopropylate; methanol; tert.-butylhydroperoxide; sodium tetrahydroborate; oxalyl dichloride; L-(+)-diisopropyl tartrate; 2,4,6-trichlorobenzoyl chloride; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; nickel diacetate; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; ethanol; dichloromethane; water; ethylene glycol; 3.1: Sharpless epoxidation / 4.1: Swern oxidation / 4.2: Swern oxidation / 9.1: Yamaguchi reaction / 9.2: Yamaguchi reaction;
DOI:10.1016/j.tetlet.2012.04.118

Reference yield:

: 1384271-72-0
C₂₅H₃₄O₂Si

: 1384271-82-2
C₂₃H₃₂O₆

Guidance literature:: Multi-step reaction with 5 steps

1.1: scandium tris(trifluoromethanesulfonate) / tetrahydrofuran; water / 12 h / 20 °C

2.1: camphor-10-sulfonic acid / dichloromethane / 0 - 20 °C

3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

4.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 4 h / 0 - 20 °C

4.2: 12 h / 0 - 20 °C

5.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / Reflux

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,4,6-trichlorobenzoyl chloride; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; triethylamine; scandium tris(trifluoromethanesulfonate); In tetrahydrofuran; dichloromethane; water; 4.1: Yamaguchi reaction / 4.2: Yamaguchi reaction;
DOI:10.1016/j.tetlet.2012.04.118