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Technology Process of bis(acetylC6H4C6H4)-o-carborane

bis(acetylC6H4C6H4)-o-carborane

Base Information
  • Chemical Name:bis(acetylC6H4C6H4)-o-carborane
  • CAS No.:88519-52-2
  • Molecular Formula:C30H32B10O2
  • Molecular Weight:532.693
  • Hs Code.:
bis(acetylC<sub>6</sub>H<sub>4</sub>C<sub>6</sub>H<sub>4</sub>)-o-carborane

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Chemical Property of bis(acetylC6H4C6H4)-o-carborane
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Technology Process of bis(acetylC6H4C6H4)-o-carborane

There total 1 articles about bis(acetylC6H4C6H4)-o-carborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2-bis-(diphenyl)-o-carborane
84350-70-9

1,2-bis-(diphenyl)-o-carborane

bis(acetylC<sub>6</sub>H<sub>4</sub>C<sub>6</sub>H<sub>4</sub>)-o-carborane
88519-52-2

bis(acetylC6H4C6H4)-o-carborane

Guidance literature:
With aluminium trichloride; acetyl chloride; In not given; according to: V. N. Kalinin et al., Dokl. Akad. Nauk SSSR, 236, No. 2, 367-370 (1977).; elem. anal.;

Reference yield: 50.0%

bis(acetylC<sub>6</sub>H<sub>4</sub>C<sub>6</sub>H<sub>4</sub>)-o-carborane
88519-52-2

bis(acetylC6H4C6H4)-o-carborane

C<sub>6</sub>H<sub>3</sub>(C<sub>6</sub>H<sub>5</sub>)(C<sub>6</sub>H<sub>4</sub>)2C<sub>2</sub>B<sub>10</sub>H<sub>10</sub>(C<sub>6</sub>H<sub>4</sub>)2

C6H3(C6H5)(C6H4)2C2B10H10(C6H4)2

Guidance literature:
With hydrogenchloride; orthoformic acid triethyl ester; acetophenone; In not given; react. of acetophenone with carborane in the presence of HC(OEt)3 by passing dry hydrogen chloride, heating at 400°C; (according to: V. N. Kalinin et al., Dokl. Akad. Nauk SSSR, 236, 367-370 (1977).); pptn. by add. of EtOH;
upstream raw materials:

1,2-bis-(diphenyl)-o-carborane

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