3-benzyloxycarbonylamino-1-propyl O-(2,4-di-O-acetyl-6-O-tert-butyldiphenylsilyl-β-D-galactopyranosyl)-(1-4)-3-O-acetyl-2-acetamido-6-O-tert-butyldiphenylsilyl-2-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:3-benzyloxycarbonylamino-1-propyl O-(2,4-di-O-acetyl-6-O-tert-butyldiphenylsilyl-β-D-galactopyranosyl)-(1-4)-3-O-acetyl-2-acetamido-6-O-tert-butyldiphenylsilyl-2-deoxy-β-D-glucopyranoside
CAS No.:347391-83-7
Molecular Formula:C₆₃H₈₀N₂O₁₆Si₂
Molecular Weight:1177.5
Hs Code.:

3-benzyloxycarbonylamino-1-propyl O-(2,4-di-O-acetyl-6-O-tert-butyldiphenylsilyl-β-D-galactopyranosyl)-(1-4)-3-O-acetyl-2-acetamido-6-O-tert-butyldiphenylsilyl-2-deoxy-β-D-glucopyranoside

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Chemical Property of 3-benzyloxycarbonylamino-1-propyl O-(2,4-di-O-acetyl-6-O-tert-butyldiphenylsilyl-β-D-galactopyranosyl)-(1-4)-3-O-acetyl-2-acetamido-6-O-tert-butyldiphenylsilyl-2-deoxy-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

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Technology Process of 3-benzyloxycarbonylamino-1-propyl O-(2,4-di-O-acetyl-6-O-tert-butyldiphenylsilyl-β-D-galactopyranosyl)-(1-4)-3-O-acetyl-2-acetamido-6-O-tert-butyldiphenylsilyl-2-deoxy-β-D-glucopyranoside

There total 6 articles about 3-benzyloxycarbonylamino-1-propyl O-(2,4-di-O-acetyl-6-O-tert-butyldiphenylsilyl-β-D-galactopyranosyl)-(1-4)-3-O-acetyl-2-acetamido-6-O-tert-butyldiphenylsilyl-2-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 347391-83-7
3-benzyloxycarbonylamino-1-propyl O-(2,4-di-O-acetyl-6-O-tert-butyldiphenylsilyl-β-D-galactopyranosyl)-(1-4)-3-O-acetyl-2-acetamido-6-O-tert-butyldiphenylsilyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / imidazole / dimethylformamide / 6 h / 20 °C

2: pyridinium triflate / CH₂Cl₂ / 1 h / 20 °C

3: CH₂Cl₂ / 1 h / 20 °C

4: 2.80 g / H₂O / 0.25 h / 20 °C

With 1H-imidazole; pyridinium triflate; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)00196-X

Reference yield:

: {3-[(2R,3R,4R,5S,6R)-3-Acetylamino-4-hydroxy-6-hydroxymethyl-5-((2S,3R,4S,5R,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-2-yloxy]-propyl}-carbamic acid benzyl ester

: 347391-83-7
3-benzyloxycarbonylamino-1-propyl O-(2,4-di-O-acetyl-6-O-tert-butyldiphenylsilyl-β-D-galactopyranosyl)-(1-4)-3-O-acetyl-2-acetamido-6-O-tert-butyldiphenylsilyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / imidazole / dimethylformamide / 6 h / 20 °C

2: pyridinium triflate / CH₂Cl₂ / 1 h / 20 °C

3: CH₂Cl₂ / 1 h / 20 °C

4: 2.80 g / H₂O / 0.25 h / 20 °C

With 1H-imidazole; pyridinium triflate; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)00196-X

Reference yield:

: (3-{(2R,3R,4R,5S,6R)-3-Amino-6-(tert-butyl-diphenyl-silanyloxymethyl)-5-[(2S,3R,4S,5R,6R)-6-(tert-butyl-diphenyl-silanyloxymethyl)-3,4,5-trihydroxy-tetrahydro-pyran-2-yloxy]-4-hydroxy-tetrahydro-pyran-2-yloxy}-propyl)-carbamic acid benzyl ester

: 347391-83-7
3-benzyloxycarbonylamino-1-propyl O-(2,4-di-O-acetyl-6-O-tert-butyldiphenylsilyl-β-D-galactopyranosyl)-(1-4)-3-O-acetyl-2-acetamido-6-O-tert-butyldiphenylsilyl-2-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 49.8 mg / methanol / 1 h / 20 °C

2: pyridinium triflate / CH₂Cl₂ / 1 h / 20 °C

3: CH₂Cl₂ / 1 h / 20 °C

4: 2.80 g / H₂O / 0.25 h / 20 °C

With pyridinium triflate; In methanol; dichloromethane; water;
DOI:10.1016/S0040-4020(01)00196-X