C₁₇H₂₆O₃Si

Base Information

Chemical Name:C₁₇H₂₆O₃Si
CAS No.:1427351-44-7
Molecular Formula:C₁₇H₂₆O₃Si
Molecular Weight:306.477
Hs Code.:

C<sub>17</sub>H<sub>26</sub>O<sub>3</sub>Si

Synonyms:

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Chemical Property of C₁₇H₂₆O₃Si

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Technology Process of C₁₇H₂₆O₃Si

There total 4 articles about C₁₇H₂₆O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 132969-60-9
(2S)-3-[(4-methoxybenzyl)oxy]-2-methylpropanal

: 1066-54-2
trimethylsilylacetylene

: 1393364-32-3
(3S,4S)-5-(4-methoxybenzyloxy)-4-methyl-1-(trimethylsilyl)pent-1-yn-3-ol

: 1427351-44-7
C₁₇H₂₆O₃Si

Guidance literature:: trimethylsilylacetylene; With diethylzinc; In toluene; for 1h; Inert atmosphere; Schlenk technique; Reflux;

With titanium(IV) isopropylate; (R)-1,1'-Bi-2-naphthol; In diethyl ether; toluene; at 23 ℃; for 1h; Inert atmosphere; Schlenk technique;

(2S)-3-[(4-methoxybenzyl)oxy]-2-methylpropanal; In diethyl ether; toluene; Overall yield = 80 %; Overall yield = 185 mg; Inert atmosphere; Schlenk technique;
DOI:10.1039/c2ob26906f

Reference yield:

: 89238-99-3
O-(4-methoxybenzyl)-trichloroacetimidate

: 1427351-44-7
C₁₇H₂₆O₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: camphor-10-sulfonic acid / dichloromethane / 16 h / Inert atmosphere; Schlenk technique

2.1: diisobutylaluminium hydride / dichloromethane / 4.42 h / -78 °C / Inert atmosphere; Schlenk technique

3.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 23 °C / Inert atmosphere; Schlenk technique

4.1: diethylzinc / toluene / 1 h / Inert atmosphere; Schlenk technique; Reflux

4.2: 1 h / 23 °C / Inert atmosphere; Schlenk technique

4.3: Inert atmosphere; Schlenk technique

With camphor-10-sulfonic acid; diethylzinc; diisobutylaluminium hydride; Dess-Martin periodane; In dichloromethane; toluene;
DOI:10.1039/c2ob26906f

Reference yield:

: 132969-71-2
methyl (2S)-[(4-methoxybenzyl)oxy]-2-methylpropanoate

: 1427351-44-7
C₁₇H₂₆O₃Si

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / dichloromethane / 4.42 h / -78 °C / Inert atmosphere; Schlenk technique

2.1: Dess-Martin periodane / dichloromethane / 3 h / 0 - 23 °C / Inert atmosphere; Schlenk technique

3.1: diethylzinc / toluene / 1 h / Inert atmosphere; Schlenk technique; Reflux

3.2: 1 h / 23 °C / Inert atmosphere; Schlenk technique

3.3: Inert atmosphere; Schlenk technique

With diethylzinc; diisobutylaluminium hydride; Dess-Martin periodane; In dichloromethane; toluene;
DOI:10.1039/c2ob26906f