C₄₂H₅₁N₄O₈PS

Base Information

Chemical Name:C₄₂H₅₁N₄O₈PS
CAS No.:1352230-41-1
Molecular Formula:C₄₂H₅₁N₄O₈PS
Molecular Weight:802.929
Hs Code.:

C<sub>42</sub>H<sub>51</sub>N<sub>4</sub>O<sub>8</sub>PS

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Chemical Property of C₄₂H₅₁N₄O₈PS

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Technology Process of C₄₂H₅₁N₄O₈PS

There total 17 articles about C₄₂H₅₁N₄O₈PS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3-O-(naphthalene-2-ylmethyl)-1,2;5,6-0-di(isopropylidene)-α-D-allofuranose

: 1352230-41-1
C₄₂H₅₁N₄O₈PS

Guidance literature:: Multi-step reaction with 16 steps

1.1: water; acetic acid / 16 h / 20 °C

2.1: sodium periodate / 1,4-dioxane; water / 1.67 h

3.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 °C / Cooling with ice

4.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

5.2: 1 h / -78 - 20 °C

6.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

6.2: 3 h / -78 °C

6.3: 20 °C

7.1: sulfuric acid / 2 h / 20 °C

8.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1.5 h / 55 °C

8.2: 0 - 60 °C

9.1: potassium carbonate / methanol / 96 h / 20 °C

9.2: 12 h / 0 °C

10.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / 20 °C

10.2: 1.5 h

11.1: pyridine / 5.5 h / 0 - 20 °C

12.1: potassium thioacetate / N,N-dimethyl-formamide / 4 h / 20 °C

12.2: 12 h

13.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 3.5 h

14.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h

15.1: pyridine / 6.5 h / 0 - 20 °C

16.1: 1H-tetrazole; 1-methyl-1H-imidazole / N,N-dimethyl-formamide / 5 h / 20 °C

With pyridine; 1-methyl-1H-imidazole; 1H-tetrazole; sodium periodate; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; tetrabutyl ammonium fluoride; water; potassium carbonate; acetic acid; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; potassium thioacetate; sulfuric acid; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1057385-93-9
(3aR,5S,6R,6aR)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[3,2-d][1,3]dioxole-5-carbaldehyde

: 1352230-41-1
C₄₂H₅₁N₄O₈PS

Guidance literature:: Multi-step reaction with 14 steps

1.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 °C / Cooling with ice

2.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

3.2: 1 h / -78 - 20 °C

4.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

4.2: 3 h / -78 °C

4.3: 20 °C

5.1: sulfuric acid / 2 h / 20 °C

6.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1.5 h / 55 °C

6.2: 0 - 60 °C

7.1: potassium carbonate / methanol / 96 h / 20 °C

7.2: 12 h / 0 °C

8.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / 20 °C

8.2: 1.5 h

9.1: pyridine / 5.5 h / 0 - 20 °C

10.1: potassium thioacetate / N,N-dimethyl-formamide / 4 h / 20 °C

10.2: 12 h

11.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 3.5 h

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h

13.1: pyridine / 6.5 h / 0 - 20 °C

14.1: 1H-tetrazole; 1-methyl-1H-imidazole / N,N-dimethyl-formamide / 5 h / 20 °C

With pyridine; 1-methyl-1H-imidazole; 1H-tetrazole; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; tetrabutyl ammonium fluoride; water; potassium carbonate; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; potassium thioacetate; sulfuric acid; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 620630-82-2
1,2 5,6-O-di(isopropylidene)-α-D-allofuranose

: 1352230-41-1
C₄₂H₅₁N₄O₈PS

Guidance literature:: Multi-step reaction with 17 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / Cooling with ice

2.1: water; acetic acid / 16 h / 20 °C

3.1: sodium periodate / 1,4-dioxane; water / 1.67 h

4.1: sodium hydroxide; water / tetrahydrofuran / 72 h / 20 °C / Cooling with ice

5.1: triethylamine / dichloromethane / 16 h / 0 - 20 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

6.2: 1 h / -78 - 20 °C

7.1: cerium(III) chloride / tetrahydrofuran / 1.58 h / 0 °C

7.2: 3 h / -78 °C

7.3: 20 °C

8.1: sulfuric acid / 2 h / 20 °C

9.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 1.5 h / 55 °C

9.2: 0 - 60 °C

10.1: potassium carbonate / methanol / 96 h / 20 °C

10.2: 12 h / 0 °C

11.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 2 h / 20 °C

11.2: 1.5 h

12.1: pyridine / 5.5 h / 0 - 20 °C

13.1: potassium thioacetate / N,N-dimethyl-formamide / 4 h / 20 °C

13.2: 12 h

14.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 3.5 h

15.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h

16.1: pyridine / 6.5 h / 0 - 20 °C

17.1: 1H-tetrazole; 1-methyl-1H-imidazole / N,N-dimethyl-formamide / 5 h / 20 °C

With pyridine; 1-methyl-1H-imidazole; 1H-tetrazole; sodium periodate; N,O-bis-(trimethylsilyl)-acetamide; cerium(III) chloride; oxalyl dichloride; tetrabutyl ammonium fluoride; water; sodium hydride; potassium carbonate; acetic acid; dimethyl sulfoxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; potassium thioacetate; sulfuric acid; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;