1-amino-6-benzyloxy-5-methoxyindan

Base Information

Chemical Name:1-amino-6-benzyloxy-5-methoxyindan
CAS No.:64974-57-8
Molecular Formula:C₃₅H₃₇NO₅
Molecular Weight:551.682
Hs Code.:

1-<N-(3-Acetoxy-4-benzyloxyphenethyl)-N-methyl>amino-6-benzyloxy-5-methoxyindan

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-amino-6-benzyloxy-5-methoxyindan

Chemical Property:

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Technology Process of 1-amino-6-benzyloxy-5-methoxyindan

There total 8 articles about 1-amino-6-benzyloxy-5-methoxyindan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: [2-(3-Acetoxy-4-benzyloxy-phenyl)-ethyl]-[6-benzyloxy-5-methoxy-indan-(1E)-ylidene]-methyl-ammonium; iodide

: 64974-57-8
1-amino-6-benzyloxy-5-methoxyindan

Guidance literature:: With sodium tetrahydroborate; In methanol;
DOI:10.1248/cpb.25.1129

Reference yield:

: 4049-39-2
4-benzyloxy-3-hydroxy-benzaldehyde

: 64974-57-8
1-amino-6-benzyloxy-5-methoxyindan

Guidance literature:: Multi-step reaction with 8 steps

1: (i) NaH, benzene, (ii) /BRN= 505943/

2: MeNH₂ / ethanol

3: LiAlH₄ / tetrahydrofuran

4: 170 - 180 °C

5: aq. HCl / methanol

6: Et₃N / CHCl₃

7: (i) POCl₃, MeCN, (ii) /BRN= 969135/

8: NaBH₄ / methanol

With hydrogenchloride; sodium tetrahydroborate; lithium aluminium tetrahydride; triethylamine; methylamine; In tetrahydrofuran; methanol; ethanol; chloroform;
DOI:10.1248/cpb.25.1129

Reference yield:

: 64974-45-4
4-(benzyloxy)-3-(methoxymethoxy)benzaldehyde

: 64974-57-8
1-amino-6-benzyloxy-5-methoxyindan

Guidance literature:: Multi-step reaction with 7 steps

1: MeNH₂ / ethanol

2: LiAlH₄ / tetrahydrofuran

3: 170 - 180 °C

4: aq. HCl / methanol

5: Et₃N / CHCl₃

6: (i) POCl₃, MeCN, (ii) /BRN= 969135/

7: NaBH₄ / methanol

With hydrogenchloride; sodium tetrahydroborate; lithium aluminium tetrahydride; triethylamine; methylamine; In tetrahydrofuran; methanol; ethanol; chloroform;
DOI:10.1248/cpb.25.1129