(5S,6S)-1-Amino-6-cyclohexylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-2,5-diol

Base Information

Chemical Name:(5S,6S)-1-Amino-6-cyclohexylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-2,5-diol
CAS No.:60056-51-1
Molecular Formula:C₁₇H₂₆N₂O₂
Molecular Weight:290.406
Hs Code.:

Synonyms:

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Chemical Property of (5S,6S)-1-Amino-6-cyclohexylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-2,5-diol

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Technology Process of (5S,6S)-1-Amino-6-cyclohexylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-2,5-diol

There total 7 articles about (5S,6S)-1-Amino-6-cyclohexylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-2,5-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60055-30-3
2-Hydroxy-1-nitro-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-on

: 60056-51-1
(5S,6S)-1-Amino-6-cyclohexylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-2,5-diol

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate; potassium iodide / methanol / Heating

2: hydrogenchloride; ethanol; isopentyl nitrite / tetrahydrofuran; diethyl ether / 0 °C

3: hydrogen / nickel / acetic acid / 760 Torr / Ambient temperature

4: sodium tetrahydroborate / ethanol

5: sodium hydroxide / ethanol / Heating

6: (i) HCl, EtOH, xylene, (ii) H₂, Pd-C, PtO₂, MeOH

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; ethanol; hydrogen; potassium carbonate; potassium iodide; isopentyl nitrite; nickel; In tetrahydrofuran; methanol; diethyl ether; ethanol; acetic acid;

Reference yield:

: 60055-31-4
2-Benzyloxy-1-nitro-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-on

: 60056-51-1
(5S,6S)-1-Amino-6-cyclohexylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-2,5-diol

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogenchloride; ethanol; isopentyl nitrite / tetrahydrofuran; diethyl ether / 0 °C

2: hydrogen / nickel / acetic acid / 760 Torr / Ambient temperature

3: sodium tetrahydroborate / ethanol

4: sodium hydroxide / ethanol / Heating

5: (i) HCl, EtOH, xylene, (ii) H₂, Pd-C, PtO₂, MeOH

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; ethanol; hydrogen; isopentyl nitrite; nickel; In tetrahydrofuran; diethyl ether; ethanol; acetic acid;

Reference yield:

: 60055-34-7
2-Benzyloxy-1-nitro-8,9-dihydro-7H-benzocycloheptene-5,6-dione 6-oxime

: 60056-51-1
(5S,6S)-1-Amino-6-cyclohexylamino-6,7,8,9-tetrahydro-5H-benzocycloheptene-2,5-diol

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogen / nickel / acetic acid / 760 Torr / Ambient temperature

2: sodium tetrahydroborate / ethanol

3: sodium hydroxide / ethanol / Heating

4: (i) HCl, EtOH, xylene, (ii) H₂, Pd-C, PtO₂, MeOH

With sodium hydroxide; sodium tetrahydroborate; hydrogen; nickel; In ethanol; acetic acid;