Os3(CO)9(CNCH2Ph){μ-bis(diphenylphosphino)methane}

Base Information

Chemical Name:Os3(CO)9(CNCH2Ph){μ-bis(diphenylphosphino)methane}
CAS No.:154070-78-7
Molecular Formula:C₄₂H₂₉NO₉Os₃P₂
Molecular Weight:1324.24
Hs Code.:

Synonyms:

Suppliers and Price of Os3(CO)9(CNCH2Ph){μ-bis(diphenylphosphino)methane}

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Os3(CO)9(CNCH2Ph){μ-bis(diphenylphosphino)methane}

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Os3(CO)9(CNCH2Ph){μ-bis(diphenylphosphino)methane}

There total 1 articles about Os3(CO)9(CNCH2Ph){μ-bis(diphenylphosphino)methane} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 184695-96-3
Os₃(CO)10(CNCH₂C₆H₅)(NCCH₃)

: 2071-20-7
bis-diphenylphosphinomethane

: 154070-78-7
Os3(CO)9(CNCH2Ph){μ-bis(diphenylphosphino)methane}

Guidance literature:: In dichloromethane; Treating CH2Cl2 soln. of Os3-compd. with dppm and stirring.; Removal of solvent under vac., chromy. of residue on silica gel TLC plate, elem. anal.;

Reference yield: 58.0%

: 154070-78-7
Os3(CO)9(CNCH2Ph){μ-bis(diphenylphosphino)methane}

: (μ-H)2Os3(CO)7(CNCH2Ph){μ3-η4-(diphenylphosphino)CHP(Ph)C6H4}

Guidance literature:: In toluene; Thermolysis of starting compd. in refluxing toluene results in a color change from orange to green in 3 h; react. is continued for another 5 h.; Color changes again to orange on cooling. Removal of solvent under vac., chromy. of residue on silica gel TLC plate with Et2O/hexane as eluent, elem. anal.;

Reference yield:

: 154070-78-7
Os3(CO)9(CNCH2Ph){μ-bis(diphenylphosphino)methane}

: (μ-H)Os3(CO)6(PPh3){(diphenylphosphino)CH2P(Ph)C6H4CNCH2Ph}

Guidance literature:: With P(C₆H₅)3; In toluene; Thermolysis of Os3-compd. with PPh3 in refluxing toluene for 3 h is accompanied by a color change to deep orange.; Removal of solvent under vac., chromy. of residue on silica gel TLC plate with CH2Cl2/hexane as eluent, elem. anal.;