C₂₅H₂₅ClN₂O₃

Base Information

Chemical Name:C₂₅H₂₅ClN₂O₃
CAS No.:603122-43-6
Molecular Formula:C₂₅H₂₅ClN₂O₃
Molecular Weight:436.938
Hs Code.:

C<sub>25</sub>H<sub>25</sub>ClN<sub>2</sub>O<sub>3</sub>

Synonyms:

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Chemical Property of C₂₅H₂₅ClN₂O₃

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Technology Process of C₂₅H₂₅ClN₂O₃

There total 10 articles about C₂₅H₂₅ClN₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 132990-84-2
(2S)-N-benzyl-7-methoxy-1,2,3,4-tetrahydronaphthalen-2-amine

: 603122-43-6
C₂₅H₂₅ClN₂O₃

Guidance literature:: Multi-step reaction with 7 steps

1: boron tribromide / dichloromethane / 4 - 20 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / methanol / 2 h

3: sodium hydroxide / tetrahydrofuran; water / 1 h / 20 °C / pH 7 - 8

4: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

5: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water / 2 h / 20 - 80 °C / Inert atmosphere

6: palladium 10% on activated carbon; hydrogen / methanol / 1 h

7: ethanol / Reflux

With 2,6-dimethylpyridine; sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; hydrogen; boron tribromide; sodium carbonate; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 5: Suzuki coupling;
DOI:10.1021/jm800222k

Reference yield:

: 603122-70-9
(7S)-7-(benzylamino)-5,6,7,8-tetrahydronaphthalen-2-ol

: 603122-43-6
C₂₅H₂₅ClN₂O₃

Guidance literature:: Multi-step reaction with 6 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 2 h

2: sodium hydroxide / tetrahydrofuran; water / 1 h / 20 °C / pH 7 - 8

3: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

4: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water / 2 h / 20 - 80 °C / Inert atmosphere

5: palladium 10% on activated carbon; hydrogen / methanol / 1 h

6: ethanol / Reflux

With 2,6-dimethylpyridine; sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; hydrogen; sodium carbonate; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; 4: Suzuki coupling;
DOI:10.1021/jm800222k

Reference yield:

: 194785-39-2
benzyl [(2S)-7-hydroxy-1,2,3,4-tetrahydronaphthalen-2-yl]carbamate

: 603122-43-6
C₂₅H₂₅ClN₂O₃

Guidance literature:: Multi-step reaction with 4 steps

1: 2,6-dimethylpyridine / dichloromethane / 1 h / -78 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water / 2 h / 20 - 80 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol / 1 h

4: ethanol / Reflux

With 2,6-dimethylpyridine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; hydrogen; sodium carbonate; In methanol; ethanol; dichloromethane; water; 2: Suzuki coupling;
DOI:10.1021/jm800222k