1,1-dimethylethyl amino>-2,3-O-(1-methylethylidene)-β-D-ribo-dec-5-enofuranosid>uronates

Base Information

Chemical Name:1,1-dimethylethyl amino>-2,3-O-(1-methylethylidene)-β-D-ribo-dec-5-enofuranosid>uronates
CAS No.:124288-78-4
Molecular Formula:C₂₅H₃₈N₂O₉S
Molecular Weight:542.651
Hs Code.:

1,1-dimethylethyl <methyl-6-hydroximino-5,6,7,8,9-pentadeoxy-9(S)-<<(4-methylphenyl)sulfonyl>amino>-2,3-O-(1-methylethylidene)-β-D-ribo-dec-5-enofuranosid>uronates

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Chemical Property of 1,1-dimethylethyl amino>-2,3-O-(1-methylethylidene)-β-D-ribo-dec-5-enofuranosid>uronates

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Technology Process of 1,1-dimethylethyl amino>-2,3-O-(1-methylethylidene)-β-D-ribo-dec-5-enofuranosid>uronates

There total 7 articles about 1,1-dimethylethyl amino>-2,3-O-(1-methylethylidene)-β-D-ribo-dec-5-enofuranosid>uronates which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 124288-77-3,124288-96-6
1,1-dimethylethyl amino>-2,3-O-(1-methyl-ethylidene)-β-D-ribo-dec-5-enofuranosid>uronates

: 124288-78-4,124288-97-7
1,1-dimethylethyl amino>-2,3-O-(1-methylethylidene)-β-D-ribo-dec-5-enofuranosid>uronates

Guidance literature:: With acetic acid; zinc; In tetrahydrofuran; at 45 ℃; for 0.25h;
DOI:10.1021/jo00290a028

Reference yield:

: 124288-73-9
1,1-dimethylethyl (S)-2-<<(4-methylphenyl)sulfonyl>-amino>-5-<<(phenylmethoxy)carbonyl>amino>pentanoate

: 124288-78-4,124288-97-7
1,1-dimethylethyl amino>-2,3-O-(1-methylethylidene)-β-D-ribo-dec-5-enofuranosid>uronates

Guidance literature:: Multi-step reaction with 5 steps

1: 99 percent / H₂ / 10percent Pd/C / methanol / 3102.9 Torr

2: 56 percent / m-CPBA / CH₂Cl₂ / 0.28 h / Heating

3: 86 percent / KF / acetonitrile / 24 h / 22 °C

4: 96 percent / dicyclohexylcarbodiimde, copper(I) chloride / acetonitrile / 16 h / 35 °C

5: 84 percent / zinc dust, acetic acid / tetrahydrofuran / 0.25 h / 45 °C

With potassium fluoride; hydrogen; acetic acid; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; copper(l) chloride; zinc; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.1021/jo00290a028

Reference yield:

: 110414-90-9
α-N-tosyl-δ-N-carbobenzoxyornthine

: 124288-78-4,124288-97-7
1,1-dimethylethyl amino>-2,3-O-(1-methylethylidene)-β-D-ribo-dec-5-enofuranosid>uronates

Guidance literature:: Multi-step reaction with 6 steps

1: 82 percent / CHCl₃ / 22 h / 22 °C

2: 99 percent / H₂ / 10percent Pd/C / methanol / 3102.9 Torr

3: 56 percent / m-CPBA / CH₂Cl₂ / 0.28 h / Heating

4: 86 percent / KF / acetonitrile / 24 h / 22 °C

5: 96 percent / dicyclohexylcarbodiimde, copper(I) chloride / acetonitrile / 16 h / 35 °C

6: 84 percent / zinc dust, acetic acid / tetrahydrofuran / 0.25 h / 45 °C

With potassium fluoride; hydrogen; acetic acid; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide; copper(l) chloride; zinc; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; chloroform; acetonitrile;
DOI:10.1021/jo00290a028