5-chloro-N-((1-(4-(2-oxopyridin-1(2H)-yl)phenyl)-1H-imidazol-4-yl)methyl)thiophene-2-carboxamide thiocyanate

Base Information

Chemical Name:5-chloro-N-((1-(4-(2-oxopyridin-1(2H)-yl)phenyl)-1H-imidazol-4-yl)methyl)thiophene-2-carboxamide thiocyanate
CAS No.:1313610-83-1
Molecular Formula:CHNS*C₂₀H₁₅ClN₄O₂S
Molecular Weight:469.975
Hs Code.:

Synonyms:

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Chemical Property of 5-chloro-N-((1-(4-(2-oxopyridin-1(2H)-yl)phenyl)-1H-imidazol-4-yl)methyl)thiophene-2-carboxamide thiocyanate

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Technology Process of 5-chloro-N-((1-(4-(2-oxopyridin-1(2H)-yl)phenyl)-1H-imidazol-4-yl)methyl)thiophene-2-carboxamide thiocyanate

There total 8 articles about 5-chloro-N-((1-(4-(2-oxopyridin-1(2H)-yl)phenyl)-1H-imidazol-4-yl)methyl)thiophene-2-carboxamide thiocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 142-08-5
2-hydroxypyridin

: 1313610-83-1
5-chloro-N-((1-(4-(2-oxopyridin-1(2H)-yl)phenyl)-1H-imidazol-4-yl)methyl)thiophene-2-carboxamide thiocyanate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; copper(l) iodide / dimethyl sulfoxide / 3 h / 120 °C / Industry scale

2.1: potassium carbonate; L-proline; copper(l) iodide / dimethyl sulfoxide / 3.5 h / 120 °C / Industry scale

3.1: toluene / 0.25 h / Industry scale; Inert atmosphere

3.2: 4 h / 100 °C / Industry scale

3.3: 35 °C / Industry scale

4.1: isopropyl alcohol; water / 16 h

With copper(l) iodide; potassium carbonate; L-proline; In water; dimethyl sulfoxide; isopropyl alcohol; toluene;

Reference yield:

: 624-38-4,1032416-46-8
para-diiodobenzene

: 1313610-83-1
5-chloro-N-((1-(4-(2-oxopyridin-1(2H)-yl)phenyl)-1H-imidazol-4-yl)methyl)thiophene-2-carboxamide thiocyanate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate; copper(l) iodide / dimethyl sulfoxide / 3 h / 120 °C / Industry scale

2.1: potassium carbonate; L-proline; copper(l) iodide / dimethyl sulfoxide / 3.5 h / 120 °C / Industry scale

3.1: toluene / 0.25 h / Industry scale; Inert atmosphere

3.2: 4 h / 100 °C / Industry scale

3.3: 35 °C / Industry scale

4.1: isopropyl alcohol; water / 16 h

With copper(l) iodide; potassium carbonate; L-proline; In water; dimethyl sulfoxide; isopropyl alcohol; toluene;

Reference yield:

: 766556-75-6
1-(4-iodophenyl)pyridin-2(1H)-one

: 1313610-83-1
5-chloro-N-((1-(4-(2-oxopyridin-1(2H)-yl)phenyl)-1H-imidazol-4-yl)methyl)thiophene-2-carboxamide thiocyanate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate; L-proline; copper(l) iodide / dimethyl sulfoxide / 3.5 h / 120 °C / Industry scale

2.1: toluene / 0.25 h / Industry scale; Inert atmosphere

2.2: 4 h / 100 °C / Industry scale

2.3: 35 °C / Industry scale

3.1: isopropyl alcohol; water / 16 h

With copper(l) iodide; potassium carbonate; L-proline; In water; dimethyl sulfoxide; isopropyl alcohol; toluene;