C₂₃H₂₃FN₂O₂

Base Information

Chemical Name:C₂₃H₂₃FN₂O₂
CAS No.:524734-48-3
Molecular Formula:C₂₃H₂₃FN₂O₂
Molecular Weight:378.446
Hs Code.:

C<sub>23</sub>H<sub>23</sub>FN<sub>2</sub>O<sub>2</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₂₃FN₂O₂

Chemical Property:

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Technology Process of C₂₃H₂₃FN₂O₂

There total 6 articles about C₂₃H₂₃FN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 8-(3-fluorophenyl)-1,7-naphthyridin-6-yl trifluoromethanesulfonate

: 524734-42-7
4-iodocyclohexanecarboxylic acid ethyl ester

: 524734-48-3
C₂₃H₂₃FN₂O₂

Guidance literature:: 4-iodocyclohexanecarboxylic acid ethyl ester; With chloro-trimethyl-silane; ethylene dibromide; zinc; In tetrahydrofuran; at 35 ℃; for 1.5h;

8-(3-fluorophenyl)-1,7-naphthyridin-6-yl trifluoromethanesulfonate; With 1,1'-bis-(diphenylphosphino)ferrocene; tetra-(n-butyl)ammonium iodide; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; at 35 ℃;
DOI:10.1021/jm300459a

Reference yield:

: 6635-88-7
3-(cyanomethyl)pyridine 1-oxide

: 524734-48-3
C₂₃H₂₃FN₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: N,N-Dimethylcarbamoyl chloride / toluene / 1.5 h / 80 °C

2.1: acetic acid; hydrogen bromide / 1 h / 35 °C

4.1: sodium nitrite

5.1: zinc; ethylene dibromide; chloro-trimethyl-silane / tetrahydrofuran / 1.5 h / 35 °C

5.2: 35 °C

With chloro-trimethyl-silane; hydrogen bromide; acetic acid; ethylene dibromide; N,N-Dimethylcarbamoyl chloride; zinc; sodium nitrite; In tetrahydrofuran; toluene; 3.1: |Suzuki Coupling / 5.1: |Negishi Coupling / 5.2: |Negishi Coupling;
DOI:10.1021/jm300459a

Reference yield:

: 6443-85-2
3-pyridinylacetonitrile

: 524734-48-3
C₂₃H₂₃FN₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: dihydrogen peroxide; acetic acid / 2 h / 100 °C

2.1: N,N-Dimethylcarbamoyl chloride / toluene / 1.5 h / 80 °C

3.1: acetic acid; hydrogen bromide / 1 h / 35 °C

5.1: sodium nitrite

6.1: zinc; ethylene dibromide; chloro-trimethyl-silane / tetrahydrofuran / 1.5 h / 35 °C

6.2: 35 °C

With chloro-trimethyl-silane; hydrogen bromide; dihydrogen peroxide; acetic acid; ethylene dibromide; N,N-Dimethylcarbamoyl chloride; zinc; sodium nitrite; In tetrahydrofuran; toluene; 4.1: |Suzuki Coupling / 6.1: |Negishi Coupling / 6.2: |Negishi Coupling;
DOI:10.1021/jm300459a