Technology Process of C12H8N2O6
There total 3 articles about C12H8N2O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
3-(1H-3-indolyl)-2,5-dihydro-1H-2,5-pyrroledione;
With
sodium hydroxide;
In
water; acetonitrile;
at 20 ℃;
for 0.0833333h;
With
dihydrogen peroxide;
In
water; acetonitrile;
at 20 ℃;
for 2.66667h;
DOI:10.1039/c003021j
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: methylmagnesium chloride / tetrahydrofuran
1.2: 48 h / Reflux
2.1: hydrogen; palladium / methanol / 760.05 Torr
3.1: toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene
4.1: sodium hydroxide / water; acetonitrile / 0.08 h / 20 °C
4.2: 2.67 h / 20 °C
With
hydrogen; methylmagnesium chloride; toluene-4-sulfonic acid; palladium; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide;
In
tetrahydrofuran; methanol; water; acetonitrile; benzene;
DOI:10.1039/c003021j
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: hydrogen; palladium / methanol / 760.05 Torr
2.1: toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone / benzene
3.1: sodium hydroxide / water; acetonitrile / 0.08 h / 20 °C
3.2: 2.67 h / 20 °C
With
hydrogen; toluene-4-sulfonic acid; palladium; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide;
In
methanol; water; acetonitrile; benzene;
DOI:10.1039/c003021j
