2-{3-[3-(4-{[6-({(2R)-2-hydroxy-2-[4-hydroxy-3-(hydroxymethyl)phenyl]ethyl}amino)hexyl]oxy}butyl)phenyl]-2,5-dioxo-1-imidazolidinyl}acetamide acetic acid salt

Base Information

Chemical Name:2-{3-[3-(4-{[6-({(2R)-2-hydroxy-2-[4-hydroxy-3-(hydroxymethyl)phenyl]ethyl}amino)hexyl]oxy}butyl)phenyl]-2,5-dioxo-1-imidazolidinyl}acetamide acetic acid salt
CAS No.:457658-83-2
Molecular Formula:C₂H₄O₂*C₃₀H₄₂N₄O₇
Molecular Weight:630.739
Hs Code.:

2-{3-[3-(4-{[6-({(2R)-2-hydroxy-2-[4-hydroxy-3-(hydroxymethyl)phenyl]ethyl}amino)hexyl]oxy}butyl)phenyl]-2,5-dioxo-1-imidazolidinyl}acetamide acetic acid salt

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Chemical Property of 2-{3-[3-(4-{[6-({(2R)-2-hydroxy-2-[4-hydroxy-3-(hydroxymethyl)phenyl]ethyl}amino)hexyl]oxy}butyl)phenyl]-2,5-dioxo-1-imidazolidinyl}acetamide acetic acid salt

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Technology Process of 2-{3-[3-(4-{[6-({(2R)-2-hydroxy-2-[4-hydroxy-3-(hydroxymethyl)phenyl]ethyl}amino)hexyl]oxy}butyl)phenyl]-2,5-dioxo-1-imidazolidinyl}acetamide acetic acid salt

There total 9 articles about 2-{3-[3-(4-{[6-({(2R)-2-hydroxy-2-[4-hydroxy-3-(hydroxymethyl)phenyl]ethyl}amino)hexyl]oxy}butyl)phenyl]-2,5-dioxo-1-imidazolidinyl}acetamide acetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 457655-80-0
C₂₁H₂₆BrN₃O₄

: 457658-83-2
2-{3-[3-(4-{[6-({(2R)-2-hydroxy-2-[4-hydroxy-3-(hydroxymethyl)phenyl]ethyl}amino)hexyl]oxy}butyl)phenyl]-2,5-dioxo-1-imidazolidinyl}acetamide acetic acid salt

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide

2: platinum(IV) oxide; hydrogen / ethyl acetate / Enzymatic reaction

3: water / 75 °C

With platinum(IV) oxide; hydrogen; In water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.05.064

Reference yield:

: 457634-96-7
1-(3-iodophenyl)-2,4-imidazolidinedione

: 457658-83-2
2-{3-[3-(4-{[6-({(2R)-2-hydroxy-2-[4-hydroxy-3-(hydroxymethyl)phenyl]ethyl}amino)hexyl]oxy}butyl)phenyl]-2,5-dioxo-1-imidazolidinyl}acetamide acetic acid salt

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydride / N,N-dimethyl-formamide

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

3: N,N-dimethyl-formamide

4: platinum(IV) oxide; hydrogen / ethyl acetate / Enzymatic reaction

5: water / 75 °C

With platinum(IV) oxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; hydrogen; sodium hydride; N-ethyl-N,N-diisopropylamine; In water; ethyl acetate; N,N-dimethyl-formamide; 2: Sonogashira coupling;
DOI:10.1016/j.bmc.2011.05.064

Reference yield:

: 457655-79-7
2-[3-(3-iodophenyl)-2,5-dioxo-1-imidazolidinyl]acetamide

: 457658-83-2
2-{3-[3-(4-{[6-({(2R)-2-hydroxy-2-[4-hydroxy-3-(hydroxymethyl)phenyl]ethyl}amino)hexyl]oxy}butyl)phenyl]-2,5-dioxo-1-imidazolidinyl}acetamide acetic acid salt

Guidance literature:: Multi-step reaction with 4 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

2: N,N-dimethyl-formamide

3: platinum(IV) oxide; hydrogen / ethyl acetate / Enzymatic reaction

4: water / 75 °C

With platinum(IV) oxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; hydrogen; N-ethyl-N,N-diisopropylamine; In water; ethyl acetate; N,N-dimethyl-formamide; 1: Sonogashira coupling;
DOI:10.1016/j.bmc.2011.05.064