C₂₁H₁₃BrN₄O

Base Information

Chemical Name:C₂₁H₁₃BrN₄O
CAS No.:1610051-78-9
Molecular Formula:C₂₁H₁₃BrN₄O
Molecular Weight:417.264
Hs Code.:

C<sub>21</sub>H<sub>13</sub>BrN<sub>4</sub>O

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₁₃BrN₄O

Chemical Property:

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Technology Process of C₂₁H₁₃BrN₄O

There total 3 articles about C₂₁H₁₃BrN₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1610051-93-8
C₁₆H₉Br₂N₃O

: 1692-25-7
3-pyridylboronic acid

: 1610051-78-9
C₂₁H₁₃BrN₄O

Guidance literature:: With potassium phosphate; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In 1,4-dioxane; water; at 130 ℃; for 0.666667h; Microwave irradiation;
DOI:10.1016/j.bmcl.2014.04.051 DOI:10.1016/j.bmcl.2014.04.051

Reference yield:

: 20776-50-5
2-amino-4-bromobenzoic acid

: 1610051-78-9
C₂₁H₁₃BrN₄O

Guidance literature:: Multi-step reaction with 3 steps

1: sodium nitrite; hydrogenchloride; tin(ll) chloride / 2 h / -5 - 20 °C

2: acetic acid / 0.08 h / 150 °C / Microwave irradiation

3: palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium phosphate / 1,4-dioxane; water / 0.67 h / 130 °C / Microwave irradiation

With hydrogenchloride; potassium phosphate; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; acetic acid; tin(ll) chloride; sodium nitrite; In 1,4-dioxane; water; 3: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.04.051

Reference yield:

: 4-bromo-2-hydrazineylbenzoic acid

: 1610051-78-9
C₂₁H₁₃BrN₄O

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 0.08 h / 150 °C / Microwave irradiation

2: palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium phosphate / 1,4-dioxane; water / 0.67 h / 130 °C / Microwave irradiation

With potassium phosphate; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; acetic acid; In 1,4-dioxane; water; 2: |Suzuki Coupling;
DOI:10.1016/j.bmcl.2014.04.051