2-Brom-3-methoxy-2,4-diphenyl-cyclobutenon

Base Information

• Chemical Name: 2-Brom-3-methoxy-2,4-diphenyl-cyclobutenon
• CAS No.: 93259-43-9
• Molecular Formula: C₁₇H₁₃BrO₂
• Molecular Weight: 329.193
• Mol file: 93259-43-9.mol

Synonyms:

Chemical Property of 2-Brom-3-methoxy-2,4-diphenyl-cyclobutenon

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-Brom-3-methoxy-2,4-diphenyl-cyclobutenon

There total 3 articles about 2-Brom-3-methoxy-2,4-diphenyl-cyclobutenon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-diphenyl-3-hydroxycyclobuten-1-one (4683-17-4) → 2-Brom-3-methoxy-2,4-diphenyl-cyclobutenon (93259-43-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Br₂

With bromine;

DOI:10.1021/ja00904a046

Reference yield:

2,4-Diphenyl-3-phenylacetoxy-cyclobuten-(2)-on-(1) (4683-16-3) → 2-Brom-3-methoxy-2,4-diphenyl-cyclobutenon (93259-43-9)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. NaOH

2: Br₂

With sodium hydroxide; bromine;

DOI:10.1021/ja00904a046

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + 2-Brom-3-hydroxy-2,4-diphenyl-cyclobuten-(3)-on-(1) (92796-42-4) → 2-Brom-3-methoxy-2,4-diphenyl-cyclobutenon (93259-43-9)

Guidance literature:

DOI:10.1021/ja00904a046

upstream raw materials:

diazomethane

2-Brom-3-hydroxy-2,4-diphenyl-cyclobuten-⁽³⁾-on-⁽¹⁾

2,4-diphenyl-3-hydroxycyclobuten-1-one

2,4-Diphenyl-3-phenylacetoxy-cyclobuten-⁽²⁾-on-⁽¹⁾