Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-pyran-2-ylmethyl ester

Base Information

Chemical Name:Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-pyran-2-ylmethyl ester
CAS No.:163959-17-9
Molecular Formula:C₄₃H₆₃N₂O₇PSi
Molecular Weight:779.042
Hs Code.:

Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-pyran-2-ylmethyl ester

Synonyms:

Suppliers and Price of Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-pyran-2-ylmethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-pyran-2-ylmethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-pyran-2-ylmethyl ester

There total 1 articles about Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-pyran-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 124482-92-4,89992-70-1
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

: 163854-66-8
[(2S,3S,4R,5R,6R)-3,4,5-Tris-benzyloxy-6-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-pyran-2-yl]-methanol

: 163959-17-9,163854-67-9,183071-96-7
Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-pyran-2-ylmethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 25 ℃; for 0.0833333h;
DOI:10.1016/0040-4039(95)00121-R

Reference yield:

: C₁₀₁H₁₀₆N₂O₂₃P₂

: 163959-17-9,163854-67-9,183071-96-7
Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-pyran-2-ylmethyl ester

: C₁₃₈H₁₅₄N₃O₃₁P₃Si

Guidance literature:: With 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction; 1.) 20 min., CH₂Cl₂, 25 deg C; 2.) 5 min., CH₂Cl₂;
DOI:10.1016/0040-4039(95)00121-R

Reference yield:

: Naphthalene-2-carboxylic acid (2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-hydroxymethyl-tetrahydro-pyran-2-ylmethyl ester

: 163959-17-9,163854-67-9,183071-96-7
Diisopropyl-phosphoramidous acid 2-cyano-ethyl ester (2S,3S,4S,5R,6R)-3,4,5-tris-benzyloxy-6-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-pyran-2-ylmethyl ester

: C₇₆H₈₆NO₁₅PSi

Guidance literature:: With 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; Yield given. Multistep reaction; 1.) 20 min., CH₂Cl₂, 25 deg C; 2.) 5 min., CH₂Cl₂;
DOI:10.1016/0040-4039(95)00121-R