3-<4-(β-D-galactopyranosyloxy)phenoxy>propylamine

Base Information

Chemical Name:3-<4-(β-D-galactopyranosyloxy)phenoxy>propylamine
CAS No.:104652-35-9
Molecular Formula:C₁₅H₂₃NO₇
Molecular Weight:329.35
Hs Code.:

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Chemical Property of 3-<4-(β-D-galactopyranosyloxy)phenoxy>propylamine

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Technology Process of 3-<4-(β-D-galactopyranosyloxy)phenoxy>propylamine

There total 3 articles about 3-<4-(β-D-galactopyranosyloxy)phenoxy>propylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90816-84-5
1-benzyloxy-4-(3-phthalimidopropoxy)benzene

: 104652-35-9
3-<4-(β-D-galactopyranosyloxy)phenoxy>propylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / H₂ / 20percent Pd on charcoal / ethyl acetate / 1 h / 2068.6 Torr

2: 14 percent / K₂CO₃ / acetone / 1) 58 deg C, 48 h, 2) r.t., overnight

3: 1) hydrazine hydrate, 2) conc. NH₄OH / 1) 95percent EtOH, reflux, 3 h, 2) CH₃OH

With ammonium hydroxide; hydrogen; potassium carbonate; hydrazine hydrate; palladium on activated charcoal; In ethyl acetate; acetone;
DOI:10.1002/jhet.5570230265

Reference yield:

: 90816-85-6
N-<3-(4-hydroxyphenoxy)propyl>phthalimide

: 104652-35-9
3-<4-(β-D-galactopyranosyloxy)phenoxy>propylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 14 percent / K₂CO₃ / acetone / 1) 58 deg C, 48 h, 2) r.t., overnight

2: 1) hydrazine hydrate, 2) conc. NH₄OH / 1) 95percent EtOH, reflux, 3 h, 2) CH₃OH

With ammonium hydroxide; potassium carbonate; hydrazine hydrate; In acetone;
DOI:10.1002/jhet.5570230265

Reference yield:

: 104652-33-7
N-<3-<4-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyloxy)phenoxy>propyl>phthalimide

: 104652-35-9
3-<4-(β-D-galactopyranosyloxy)phenoxy>propylamine

Guidance literature:: With ammonium hydroxide; hydrazine hydrate; Yield given. Multistep reaction; 1) 95percent EtOH, reflux, 3 h, 2) CH₃OH;
DOI:10.1002/jhet.5570230265