C₃₆H₄₀O₅

Base Information

• Chemical Name: C₃₆H₄₀O₅
• CAS No.: 1379520-02-1
• Molecular Formula: C₃₆H₄₀O₅
• Molecular Weight: 552.711
• Mol file: 1379520-02-1.mol

Synonyms:

Chemical Property of C₃₆H₄₀O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₆H₄₀O₅

There total 10 articles about C₃₆H₄₀O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.5%

C39H46O6 (1379520-09-8) → C36H40O5 (1379520-02-1)

Guidance literature:

With sodium hydride; In toluene; for 0.0833333h; Reflux;

DOI:10.1246/cl.2012.244

Reference yield:

C17H25IO2 (1375003-41-0) → C36H40O5 (1379520-02-1)

Guidance literature:

Multi-step reaction with 5 steps

1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / 24 h / 80 °C

2: sodium hydride / toluene / 0.17 h / 110 °C

3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / 20 °C

4: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / Reflux

5: sodium hydride / toluene / 0.08 h / Reflux

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium hydride; triethylamine; triphenylphosphine; In toluene;

DOI:10.1246/cl.2012.244

Reference yield:

C22H32O3 (1375003-42-1) → C36H40O5 (1379520-02-1)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium hydride / toluene / 0.17 h / 110 °C

2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / 20 °C

3: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine; triphenylphosphine / Reflux

4: sodium hydride / toluene / 0.08 h / Reflux

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; sodium hydride; triethylamine; triphenylphosphine; In toluene;

DOI:10.1246/cl.2012.244

upstream raw materials:

C₁₅H₁₄BrIO₃

C₃₄H₃₉BrO₅

C₃₉H₄₆O₆

C₁₇H₂₅IO₂

Refernces