Technology Process of C17H17BrN2O
There total 7 articles about C17H17BrN2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydroxide / water
1.3: 215 °C
2.1: trichlorophosphate / N,N-dimethyl-formamide
3.1: ammonium acetate
4.1: lithium aluminium tetrahydride
With
lithium aluminium tetrahydride; ammonium acetate; sodium hydroxide; trichlorophosphate;
In
water; N,N-dimethyl-formamide;
3.1: Henry reaction;
DOI:10.1002/chem.201103605
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium methylate / methanol
1.2: 160 °C
2.1: sodium hydroxide / water
2.3: 215 °C
3.1: trichlorophosphate / N,N-dimethyl-formamide
4.1: ammonium acetate
5.1: lithium aluminium tetrahydride
With
lithium aluminium tetrahydride; ammonium acetate; sodium methylate; sodium hydroxide; trichlorophosphate;
In
methanol; water; N,N-dimethyl-formamide;
1.1: Hemetsberger indole cyclization / 4.1: Henry reaction;
DOI:10.1002/chem.201103605
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium carbonate
2.1: sodium methylate / methanol
2.2: 160 °C
3.1: sodium hydroxide / water
3.3: 215 °C
4.1: trichlorophosphate / N,N-dimethyl-formamide
5.1: ammonium acetate
6.1: lithium aluminium tetrahydride
With
lithium aluminium tetrahydride; ammonium acetate; sodium methylate; potassium carbonate; sodium hydroxide; trichlorophosphate;
In
methanol; water; N,N-dimethyl-formamide;
2.1: Hemetsberger indole cyclization / 5.1: Henry reaction;
DOI:10.1002/chem.201103605
