C₃₀H₃₃NO₆

Base Information

• Chemical Name: C₃₀H₃₃NO₆
• CAS No.: 1393342-85-2
• Molecular Formula: C₃₀H₃₃NO₆
• Molecular Weight: 503.595
• Mol file: 1393342-85-2.mol

Synonyms:

Chemical Property of C₃₀H₃₃NO₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₃₃NO₆

There total 4 articles about C₃₀H₃₃NO₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C45H63NO9 → C30H33NO6 (1393342-85-2)

Guidance literature:

With water; trifluoroacetic acid; In dichloromethane; at 40 ℃; for 72h;

DOI:10.1021/jo300799s

Reference yield:

4-(bromomethyl)benzaldehyde (51359-78-5) → C30H33NO6 (1393342-85-2)

Guidance literature:

Multi-step reaction with 3 steps

1.1: toluene-4-sulfonic acid / toluene / 4 h / Reflux

2.1: sodium hydride / tetrahydrofuran; mineral oil / 20 °C / Inert atmosphere

2.2: 24.5 h / 20 °C / Inert atmosphere

3.1: water; trifluoroacetic acid / dichloromethane / 72 h / 40 °C

With water; sodium hydride; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; toluene; mineral oil;

DOI:10.1021/jo300799s

Reference yield:

4-(hydroxymethyl)benzaldehyde diethyl acetal (125734-44-3) → C30H33NO6 (1393342-85-2)

Guidance literature:

Multi-step reaction with 4 steps

1.1: water; hydrogen bromide / 1 h / Reflux

2.1: toluene-4-sulfonic acid / toluene / 4 h / Reflux

3.1: sodium hydride / tetrahydrofuran; mineral oil / 20 °C / Inert atmosphere

3.2: 24.5 h / 20 °C / Inert atmosphere

4.1: water; trifluoroacetic acid / dichloromethane / 72 h / 40 °C

With water; hydrogen bromide; sodium hydride; toluene-4-sulfonic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; toluene; mineral oil;

DOI:10.1021/jo300799s

upstream raw materials:

4-(bromomethyl)benzaldehyde

4-(hydroxymethyl)benzaldehyde diethyl acetal

2-(4-bromomethylphenyl)-5,5-dimethyl[1,3]dioxane

Refernces