(5Z,7Z,9Z)-(1S,4R,4aR,10aS)-1,2,3,4,11,11-Hexachloro-6,9-bis-(4-methoxy-phenyl)-7,8-diphenyl-1,4,4a,10a-tetrahydro-1,4-methano-benzocyclooctene

Base Information

• Chemical Name: (5Z,7Z,9Z)-(1S,4R,4aR,10aS)-1,2,3,4,11,11-Hexachloro-6,9-bis-(4-methoxy-phenyl)-7,8-diphenyl-1,4,4a,10a-tetrahydro-1,4-methano-benzocyclooctene
• CAS No.: 77884-48-1
• Molecular Formula: C₃₉H₂₈Cl₆O₂
• Molecular Weight: 741.368

Synonyms:

Chemical Property of (5Z,7Z,9Z)-(1S,4R,4aR,10aS)-1,2,3,4,11,11-Hexachloro-6,9-bis-(4-methoxy-phenyl)-7,8-diphenyl-1,4,4a,10a-tetrahydro-1,4-methano-benzocyclooctene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (5Z,7Z,9Z)-(1S,4R,4aR,10aS)-1,2,3,4,11,11-Hexachloro-6,9-bis-(4-methoxy-phenyl)-7,8-diphenyl-1,4,4a,10a-tetrahydro-1,4-methano-benzocyclooctene

There total 1 articles about (5Z,7Z,9Z)-(1S,4R,4aR,10aS)-1,2,3,4,11,11-Hexachloro-6,9-bis-(4-methoxy-phenyl)-7,8-diphenyl-1,4,4a,10a-tetrahydro-1,4-methano-benzocyclooctene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

2,5-bis(4-methoxyphenyl)-3,4-diphenylcyclopenta-2,4-dienone (38268-21-2) + 1,6,7,8,9,9-hexachloro-endo-tricyclo<4.2.1.02.5>nona-3,7-diene (70216-50-1) → (5Z,7Z,9Z)-(1S,4R,4aR,10aS)-1,2,3,4,11,11-Hexachloro-6,9-bis-(4-methoxy-phenyl)-7,8-diphenyl-1,4,4a,10a-tetrahydro-1,4-methano-benzocyclooctene (77884-48-1) + C39H28Cl6O2 (77300-33-5) + C40H28Cl6O3 (77884-47-0)

Guidance literature:

In xylene;

DOI:10.1016/0040-4020(80)88028-8

Reference yield:

(5Z,7Z,9Z)-(1S,4R,4aR,10aS)-1,2,3,4,11,11-Hexachloro-6,9-bis-(4-methoxy-phenyl)-7,8-diphenyl-1,4,4a,10a-tetrahydro-1,4-methano-benzocyclooctene (77884-48-1) → C39H28Cl6O2 (77300-33-5) + C39H28Cl6O2 (77300-34-6)

Guidance literature:

In various solvent(s); at 137 ℃; for 6h;

DOI:10.1016/S0040-4039(01)80226-4

Reference yield:

(5Z,7Z,9Z)-(1S,4R,4aR,10aS)-1,2,3,4,11,11-Hexachloro-6,9-bis-(4-methoxy-phenyl)-7,8-diphenyl-1,4,4a,10a-tetrahydro-1,4-methano-benzocyclooctene (77884-48-1) → C39H28Cl6O2 (77300-33-5) + C39H28Cl6O2 (77300-34-6)

Guidance literature:

In neat (no solvent);

DOI:10.1039/P29860001651

upstream raw materials:

2,5-bis(4-methoxyphenyl)-3,4-diphenylcyclopenta-2,4-dienone

1,6,7,8,9,9-hexachloro-endo-tricyclo<4.2.1.0^2.5>nona-3,7-diene

Downstream raw materials:

C₃₉H₂₈Cl₆O₂

C₃₉H₂₈Cl₆O₂

C₃₉H₂₈Cl₆O₂

C₃₉H₂₈Cl₆O₂

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