C₃₁H₃₈N₂O₆

Base Information

Chemical Name:C₃₁H₃₈N₂O₆
CAS No.:1609200-16-9
Molecular Formula:C₃₁H₃₈N₂O₆
Molecular Weight:534.653
Hs Code.:

C<sub>31</sub>H<sub>38</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:

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Chemical Property of C₃₁H₃₈N₂O₆

Chemical Property:

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Technology Process of C₃₁H₃₈N₂O₆

There total 12 articles about C₃₁H₃₈N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1609200-15-8
C₃₁H₃₆N₂O₄

: 1609200-16-9
C₃₁H₃₈N₂O₆

Guidance literature:: With ruthenium trichloride; sodium periodate; cerium(III) chloride heptahydrate; In water; ethyl acetate; acetonitrile; at 0 ℃; for 0.25h; Inert atmosphere;
DOI:10.1039/c4cc01843e

Reference yield:

: 120-72-9
indole

: 1609200-16-9
C₃₁H₃₈N₂O₆

Guidance literature:: Multi-step reaction with 12 steps

1: norborn-2-ene; potassium carbonate; palladium diacetate / N,N-dimethyl acetamide / 16 h / 70 °C / Inert atmosphere

2: triethylamine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

3: toluene-4-sulfonic acid / methanol / 14 h / 20 °C / Inert atmosphere

4: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

5: potassium carbonate / N,N-dimethyl-formamide / 3 h / 50 °C / Inert atmosphere

6: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (S)-2-(2-(bis(4-trifluoromethyl-phenyl)-phosphino))-5-(4-trifluoromethyl-phenyl)-4-tert-butyl-4,5-dihydro-oxazole / tert-butyl methyl ether / 15 h / 40 °C / Inert atmosphere

7: potassium hydroxide / methanol / 3.5 h / Inert atmosphere; Reflux

8: trichlorophosphate / toluene / 0.5 h / Inert atmosphere; Reflux

9: sodium tetrahydroborate / methanol / 3 h / 0 °C / Inert atmosphere

10: triethylamine; dmap / dichloromethane / 12 h / 20 °C / Inert atmosphere

11: sodium carbonate / dichloromethane / 12 h / 20 °C / Inert atmosphere

12: cerium(III) chloride heptahydrate; sodium periodate; ruthenium trichloride / ethyl acetate; water; acetonitrile / 0.25 h / 0 °C / Inert atmosphere

With 1H-imidazole; norborn-2-ene; dmap; (S)-2-(2-(bis(4-trifluoromethyl-phenyl)-phosphino))-5-(4-trifluoromethyl-phenyl)-4-tert-butyl-4,5-dihydro-oxazole; ruthenium trichloride; sodium tetrahydroborate; sodium periodate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; cerium(III) chloride heptahydrate; iodine; palladium diacetate; sodium carbonate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; triphenylphosphine; potassium hydroxide; trichlorophosphate; In methanol; dichloromethane; tert-butyl methyl ether; N,N-dimethyl acetamide; water; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; 8: |Bischler-Napieralski Reaction;
DOI:10.1039/c4cc01843e

Reference yield:

: 1318759-39-5
2-(2-(tetrahydro-2H-pyran-2-yloxy)ethyl)-1H-indole

: 1609200-16-9
C₃₁H₃₈N₂O₆

Guidance literature:: Multi-step reaction with 11 steps

1: triethylamine; dmap / dichloromethane / 3 h / 20 °C / Inert atmosphere

2: toluene-4-sulfonic acid / methanol / 14 h / 20 °C / Inert atmosphere

3: 1H-imidazole; triphenylphosphine; iodine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

4: potassium carbonate / N,N-dimethyl-formamide / 3 h / 50 °C / Inert atmosphere

5: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol / tert-butyl methyl ether; hexane / 6 h / 40 °C

6: potassium hydroxide / methanol / 3.5 h / Inert atmosphere; Reflux

7: trichlorophosphate / toluene / 0.5 h / Inert atmosphere; Reflux

8: sodium tetrahydroborate / methanol / 3 h / 0 °C / Inert atmosphere

9: triethylamine; dmap / dichloromethane / 12 h / 20 °C / Inert atmosphere

10: sodium carbonate / dichloromethane / 12 h / 20 °C / Inert atmosphere

11: cerium(III) chloride heptahydrate; sodium periodate; ruthenium trichloride / ethyl acetate; water; acetonitrile / 0.25 h / 0 °C / Inert atmosphere

With 1H-imidazole; dmap; ruthenium trichloride; sodium tetrahydroborate; sodium periodate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; cerium(III) chloride heptahydrate; iodine; sodium carbonate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; triphenylphosphine; (S)-4-tert-butyl-2-[2-(diphenylphosphino)phenyl]-4,5-dihydro-1,3-oxazol; potassium hydroxide; trichlorophosphate; In methanol; hexane; dichloromethane; tert-butyl methyl ether; water; ethyl acetate; N,N-dimethyl-formamide; toluene; acetonitrile; 7: |Bischler-Napieralski Reaction;
DOI:10.1039/c4cc01843e