2-Furanacrolein, 5-nitro-, (7-(2,3-dihydroxypropyl)-1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydropurin-8-yl)hydrazone

Base Information

Chemical Name:2-Furanacrolein, 5-nitro-, (7-(2,3-dihydroxypropyl)-1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydropurin-8-yl)hydrazone
CAS No.:78960-59-5
Molecular Formula:C₁₇H₁₉N₇O₇
Molecular Weight:433.381
Hs Code.:

Synonyms:BRN 5191269;2-Furanacrolein, 5-nitro-, (7-(2,3-dihydroxypropyl)-1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydropurin-8-yl)hydrazone;78960-59-5;C17H19N7O7;C17-H19-N7-O7;LS-70047

Suppliers and Price of 2-Furanacrolein, 5-nitro-, (7-(2,3-dihydroxypropyl)-1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydropurin-8-yl)hydrazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-Furanacrolein, 5-nitro-, (7-(2,3-dihydroxypropyl)-1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydropurin-8-yl)hydrazone

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:753.33°C at 760 mmHg
Flash Point:409.399°C
Density:1.628g/cm³
XLogP3:-0.2
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:10
Rotatable Bond Count:7
Exact Mass:433.13459597
Heavy Atom Count:31
Complexity:758

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C2=C(C(=O)N(C1=O)C)N(C(=N2)NN=CC=CC3=CC=C(O3)[N+](=O)[O-])CC(CO)O
Isomeric SMILES:CN1C2=C(C(=O)N(C1=O)C)N(C(=N2)N/N=C/C=C/C3=CC=C(O3)[N+](=O)[O-])CC(CO)O

Technology Process of 2-Furanacrolein, 5-nitro-, (7-(2,3-dihydroxypropyl)-1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydropurin-8-yl)hydrazone

There total 2 articles about 2-Furanacrolein, 5-nitro-, (7-(2,3-dihydroxypropyl)-1,3-dimethyl-2,6-dioxo-1,2,3,6-tetrahydropurin-8-yl)hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 52661-56-0,1874-22-2
5-nitrofurylacrolein

: 78520-71-5
7-(2,3-Dihydroxypropyl)-8-hydrazinotheophylline

: 78960-59-5
7-(2,3-Dihydroxy-propyl)-1,3-dimethyl-8-{N'-[(Z)-3-(5-nitro-furan-2-yl)-prop-2-en-(Z)-ylidene]-hydrazino}-3,7-dihydro-purine-2,6-dione

Guidance literature:: With hydrogenchloride; Heating;
DOI:10.1007/BF00759472

Reference yield:

: 127988-47-0
6-hydroxymethyl-1,3-dimethyl-2,4-dioxo-1,2,3,4,6,7-hexahydrooxazolo<2,3-f>purine

: 78960-59-5
7-(2,3-Dihydroxy-propyl)-1,3-dimethyl-8-{N'-[(Z)-3-(5-nitro-furan-2-yl)-prop-2-en-(Z)-ylidene]-hydrazino}-3,7-dihydro-purine-2,6-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / 98percent hydrazine hydrate / 2-methoxy-ethanol / 5 h / Heating

2: 98 percent / aq. HCl / Heating

With hydrogenchloride; hydrazine hydrate; In 2-methoxy-ethanol;
DOI:10.1007/BF00759472