C₁₀H₁₂OSe

Base Information

• Chemical Name: C₁₀H₁₂OSe
• CAS No.: 1195710-46-3
• Molecular Formula: C₁₀H₁₂OSe
• Molecular Weight: 227.165
• Mol file: 1195710-46-3.mol

Synonyms:

Chemical Property of C₁₀H₁₂OSe

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₀H₁₂OSe

There total 1 articles about C₁₀H₁₂OSe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Phenylbutyric acid (1821-12-1) → C10H12OSe (1195710-46-3)

Guidance literature:

With woollins’ reagent; In toluene; for 2h; Reflux;

DOI:10.1021/jm300735t

Reference yield:

C10H12OSe (1195710-46-3) + 7-[(tert-butoxycarbonyl)amino]-2-methylideneheptanoic acid (1394345-64-2) → 7-[(tert-butoxycarbonyl)amino]-2-{[(4-phenylbutanoyl)-selanyl]methyl}heptanoic acid (1394345-68-6)

Guidance literature:

In toluene; at 20 - 70 ℃; for 41h;

DOI:10.1021/jm300735t

Reference yield:

C10H12OSe (1195710-46-3) + 7-[(tert-butoxycarbonyl)amino]-2-methylideneheptanoic acid (1394345-64-2) → 7-amino-2-{[(4-phenylbutanoyl)selanyl]methyl}heptanoic acid trifluoroacetate (1401516-78-6)

Guidance literature:

Multi-step reaction with 2 steps

1: toluene / 41 h / 20 - 70 °C

2: water / 1 h / 0 °C

In water; toluene;

DOI:10.1021/jm300735t

upstream raw materials:

4-Phenylbutyric acid

Downstream raw materials:

7-[(tert-butoxycarbonyl)amino]-2-{[(4-phenylbutanoyl)-selanyl]methyl}heptanoic acid

7-amino-2-{[(4-phenylbutanoyl)selanyl]methyl}heptanoic acid trifluoroacetate