4-t-butyl-1,2-dinitrrobenzene

Base Information

• Chemical Name: 4-t-butyl-1,2-dinitrrobenzene
• CAS No.: 22385-83-7
• Molecular Formula: C₁₀H₁₂N₂O₄
• Molecular Weight: 224.216
• Mol file: 22385-83-7.mol

Synonyms:

Chemical Property of 4-t-butyl-1,2-dinitrrobenzene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-t-butyl-1,2-dinitrrobenzene

There total 3 articles about 4-t-butyl-1,2-dinitrrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(2,5-di-tert-butyl-phenyl)-acetamide (23278-20-8) → 4-t-butyl-1,2-dinitrrobenzene (22385-83-7)

Guidance literature:

Multi-step reaction with 3 steps

1: HNO₃ / acetic acid; acetic anhydride

2: (alkaline hydrolysis)

3: aq. H₂O₂, (CF₃CO)2O

With dihydrogen peroxide; nitric acid; trifluoroacetic anhydride; In acetic anhydride; acetic acid;

Reference yield:

5-(tert-butyl)-2-nitroaniline (142564-53-2) → 4-t-butyl-1,2-dinitrrobenzene (22385-83-7)

Guidance literature:

With dihydrogen peroxide; trifluoroacetic anhydride;

Reference yield:

acetic acid-(5-tert-butyl-2-nitro-anilide) (6933-55-7) → 4-t-butyl-1,2-dinitrrobenzene (22385-83-7)

Guidance literature:

Multi-step reaction with 2 steps

1: (alkaline hydrolysis)

2: aq. H₂O₂, (CF₃CO)2O

With dihydrogen peroxide; trifluoroacetic anhydride;

upstream raw materials:

5-(tert-butyl)-2-nitroaniline

N-(2,5-di-tert-butyl-phenyl)-acetamide

acetic acid-(5-tert-butyl-2-nitro-anilide)

Downstream raw materials:

1-methoxy-2-nitro-4-(tert-butyl)benzene

4-(tert-butyl)-2-methoxy-1-nitrobenzen