Technology Process of tetrachloro[1,2-bis(diphenylphospino)ethane]palladium(IV)
There total 2 articles about tetrachloro[1,2-bis(diphenylphospino)ethane]palladium(IV) which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
Cl2;
In
tetrachloromethane;
a suspn. of finely powd. Pd(II) complex was suspended in dry CCl4 and rapidly stirred whilst a small excess of Cl2 was slowly bubbled in; the mixt. was stirred for 30 min;; the product was filtered off and dried in vacuo; elem. anal.;;
- Guidance literature:
-
With
Cl2;
In
tetrachloromethane;
a suspn. of finely powd. Pd(II) complex (ca. 1 mmol) was suspended in dry CCl4 and rapidly stirred whilst a small excess of Cl2 was slowly bubbled in; the mixt. was stirred for 30 min;; the product was filtered off and dried in vacuo; elem. anal.;;
- Guidance literature:
-
In
dichloromethane;
other unidentified products were obtained;;
