cis-6-(p-Tolyl)-7-hydroxy-dibenzocycloheptan-on-(5)

Base Information

Chemical Name:cis-6-(p-Tolyl)-7-hydroxy-dibenzocycloheptan-on-(5)
CAS No.:975-67-7
Molecular Formula:C₂₂H₁₈O₂
Molecular Weight:314.384
Hs Code.:

cis-6-(p-Tolyl)-7-hydroxy-dibenzo<ac>cycloheptan-on-(5)

Synonyms:

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Chemical Property of cis-6-(p-Tolyl)-7-hydroxy-dibenzocycloheptan-on-(5)

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Technology Process of cis-6-(p-Tolyl)-7-hydroxy-dibenzocycloheptan-on-(5)

There total 5 articles about cis-6-(p-Tolyl)-7-hydroxy-dibenzocycloheptan-on-(5) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: trans-6-(p-Tolyl)-7-hydroxy-dibenzocycloheptan-on-(5)

: 975-67-7,1098-53-9,100802-77-5
cis-6-(p-Tolyl)-7-hydroxy-dibenzocycloheptan-on-(5)

Guidance literature:: With silica gel; In benzene;
DOI:10.1021/jo01034a050

Reference yield:

: 573-17-1
9-bromophenanthrene

: 975-67-7,1098-53-9,100802-77-5
cis-6-(p-Tolyl)-7-hydroxy-dibenzocycloheptan-on-(5)

Guidance literature:: Multi-step reaction with 5 steps

1: (i) Mg, (ii) /BRN= 507387/

2: OsO₄, Py

3: CrO₃, Py

4: NaBH₄

5: (i) aq. NaIO₄, (ii) SiO₂

With pyridine; chromium(VI) oxide; sodium tetrahydroborate; osmium(VIII) oxide;
DOI:10.1021/jo01034a050

Reference yield:

: 975-05-3
10-hydroxy-10-(4-methylbenzyl)-phenanthren-9(10H)-one

: 975-67-7,1098-53-9,100802-77-5
cis-6-(p-Tolyl)-7-hydroxy-dibenzocycloheptan-on-(5)

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄

2: (i) aq. NaIO₄, (ii) SiO₂

With sodium tetrahydroborate;
DOI:10.1021/jo01034a050