C₅H₅FeC₅H₄CH₂PS(CH₂O)2PN₃SO(C₆H₄Cl)P(NCH₃CH₂)2

Base Information

• Chemical Name: C₅H₅FeC₅H₄CH₂PS(CH₂O)2PN₃SO(C₆H₄Cl)P(NCH₃CH₂)2
• CAS No.: 401642-99-7
• Molecular Formula: C₂₃H₂₉ClFeN₅O₃P₃S₂
• Molecular Weight: 671.868
• Mol file: 401642-99-7.mol

Synonyms:

Chemical Property of C₅H₅FeC₅H₄CH₂PS(CH₂O)2PN₃SO(C₆H₄Cl)P(NCH₃CH₂)2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅H₅FeC₅H₄CH₂PS(CH₂O)2PN₃SO(C₆H₄Cl)P(NCH₃CH₂)2

There total 1 articles about C₅H₅FeC₅H₄CH₂PS(CH₂O)2PN₃SO(C₆H₄Cl)P(NCH₃CH₂)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

(ferrocenyl)CH2P(S)(CH2OH)2 (180794-53-0) + Cl2PN3SO(C6H4Cl)P(NCH3CH2)2 (401642-94-2) → C5H5FeC5H4CH2PS(CH2O)2PN3SO(C6H4Cl)P(NCH3CH2)2 (401642-99-7)

Guidance literature:

With n-butyl lithium; In tetrahydrofuran; byproducts: LiCl; n-butyl lithium was added slowply to a stirring soln. of complex in THF at -80°C and brought to room temp. over 4 h, cooled to -80°C and a soln. of thionylphophazene in THF was added dropwise, stirred at room temp. for 10 h (N2); evapd., chromd. on silica gel (ethyl acetate-hexane), elem. anal.;

DOI:10.1016/S0022-328X(01)00939-1

upstream raw materials:

(ferrocenyl)CH₂P(S)(CH₂OH)2

Cl₂PN₃SO(C₆H₄Cl)P(NCH₃CH₂)2