methyl 8-acetoxy-7-methyl-2-naphthalene carboxylate

Base Information

Chemical Name:methyl 8-acetoxy-7-methyl-2-naphthalene carboxylate
CAS No.:1239489-71-4
Molecular Formula:C₁₅H₁₄O₄
Molecular Weight:258.274
Hs Code.:

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Chemical Property of methyl 8-acetoxy-7-methyl-2-naphthalene carboxylate

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Technology Process of methyl 8-acetoxy-7-methyl-2-naphthalene carboxylate

There total 3 articles about methyl 8-acetoxy-7-methyl-2-naphthalene carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1239489-67-8
methyl 8-acetoxy-7-methyl-5,6-dihydronaphthalene-2-carboxylate

: 1239489-71-4
methyl 8-acetoxy-7-methyl-2-naphthalene carboxylate

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; at 80 ℃; for 3h;

Reference yield:

: 116047-26-8
methyl 8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate

: 1239489-71-4
methyl 8-acetoxy-7-methyl-2-naphthalene carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisopropylamine; n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C

1.2: 1 h / 20 °C

2.1: perchloric acid / tetrachloromethane / 20 °C

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 3 h / 80 °C

With n-butyllithium; perchloric acid; diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; 1,4-dioxane; tetrachloromethane; hexane;

Reference yield:

: 1116093-69-6
methyl 7-methyl-8-oxo-5,6,7,8-tetrahydronaphthalene-2-carboxylate

: 1239489-71-4
methyl 8-acetoxy-7-methyl-2-naphthalene carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: perchloric acid / tetrachloromethane / 20 °C

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 3 h / 80 °C

With perchloric acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; tetrachloromethane;