3-Methyl-7,8,9,10-tetrahydro-6h-benzo[c]chromen-6-one

Base Information

Chemical Name:3-Methyl-7,8,9,10-tetrahydro-6h-benzo[c]chromen-6-one
CAS No.:83051-34-7
Molecular Formula:C₁₄H₁₄O₂
Molecular Weight:214.264
Hs Code.:
NSC Number:100992
DSSTox Substance ID:DTXSID70295289
Wikidata:Q82035133

Synonyms:3-methyl-7,8,9,10-tetrahydro-6h-benzo[c]chromen-6-one;83051-34-7;NSC100992;NCIOpen2_006739;SCHEMBL7532636;DTXSID70295289;NSC-100992

Suppliers and Price of 3-Methyl-7,8,9,10-tetrahydro-6h-benzo[c]chromen-6-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 3-Methyl-7,8,9,10-tetrahydro-6h-benzo[c]chromen-6-one

Chemical Property:

Vapor Pressure:2.95E-06mmHg at 25°C
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:214.099379685
Heavy Atom Count:16
Complexity:343

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=CC2=C(C=C1)C3=C(CCCC3)C(=O)O2

Technology Process of 3-Methyl-7,8,9,10-tetrahydro-6h-benzo[c]chromen-6-one

There total 4 articles about 3-Methyl-7,8,9,10-tetrahydro-6h-benzo[c]chromen-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 4'-methyl-3,4,5,6-tetrahydro-[1,1'-biphenyl]-2-carboxylic acid

: 83051-34-7
3-methyl-7,8,9,10-tetrahydro-6H-dibenzopyran-6-one

Guidance literature:: With dichloro(dimethylglyoxime)(dimethylglyoximato)cobalt(III); 9-(2-mesityl)-10-methylacridinium perchlorate; In acetonitrile; at 20 ℃; for 10h; Schlenk technique; Inert atmosphere; Irradiation;
DOI:10.1021/acs.joc.7b03195

Reference yield: 60.6%

: 108-39-4
3-methyl-phenol

: 1655-07-8
ethyl 2-oxocyclohexane carboxylate

: 83051-34-7
3-methyl-7,8,9,10-tetrahydro-6H-dibenzopyran-6-one

Guidance literature:: With sulfuric acid; at 20 ℃;
DOI:10.1248/cpb.46.1683

Reference yield: 32.0%

: C₁₄H₁₅BrO₂

: 83051-34-7
3-methyl-7,8,9,10-tetrahydro-6H-dibenzopyran-6-one

: 1-methyl-7,8,9,10-tetrahydro-6H-benzo[c]chromen-6-one

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 120 ℃; for 2h; Inert atmosphere; Sealed tube; Microwave irradiation; Green chemistry;
DOI:10.1021/acs.joc.8b00048