trans-1,4-Cyclohexanediyldimethylene bis(chloroformate)

Base Information

Chemical Name:trans-1,4-Cyclohexanediyldimethylene bis(chloroformate)
CAS No.:46744-84-7
Molecular Formula:C₁₀H₁₄Cl₂O₄
Molecular Weight:269.125
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trans-1,4-Cyclohexanediyldimethylene bis(chloroformate)

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Technology Process of trans-1,4-Cyclohexanediyldimethylene bis(chloroformate)

There total 1 articles about trans-1,4-Cyclohexanediyldimethylene bis(chloroformate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 46744-84-7
trans-1,4-Cyclohexanediyldimethylene bis(chloroformate)

Guidance literature:: 1,4-Cyclohexan-dimethanol (cis/trans-Gemisch), COCl2;

Reference yield:

: 46744-84-7
trans-1,4-Cyclohexanediyldimethylene bis(chloroformate)

: 86217-98-3
C₁₄H₂₈N₂O₂⁽²⁺⁾*2BF₄^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: 4 h / 3 - 6 °C

2: 55 percent / NaBF₄ / dimethylformamide / 2 h / Ambient temperature

With sodium tetrafluoroborate; In N,N-dimethyl-formamide;
DOI:10.1021/jo00163a047

Reference yield:

: 46744-84-7
trans-1,4-Cyclohexanediyldimethylene bis(chloroformate)

: 86218-05-5
trans-1,4-Bis(hydroxymethyl)cyclohexanediformate

Guidance literature:: Multi-step reaction with 2 steps

1: 4 h / 3 - 6 °C

2: H₂O / dimethylformamide / Ambient temperature

With water; In N,N-dimethyl-formamide;
DOI:10.1021/jo00163a047