trans-1,4-Cyclohexanediyldimethylene bis(chloroformate)

Base Information

• Chemical Name: trans-1,4-Cyclohexanediyldimethylene bis(chloroformate)
• CAS No.: 46744-84-7
• Molecular Formula: C₁₀H₁₄Cl₂O₄
• Molecular Weight: 269.125
• Mol file: 46744-84-7.mol

Synonyms:

Chemical Property of trans-1,4-Cyclohexanediyldimethylene bis(chloroformate)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of trans-1,4-Cyclohexanediyldimethylene bis(chloroformate)

There total 1 articles about trans-1,4-Cyclohexanediyldimethylene bis(chloroformate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ trans-1,4-Cyclohexanediyldimethylene bis(chloroformate) (46744-84-7)

Guidance literature:

1,4-Cyclohexan-dimethanol (cis/trans-Gemisch), COCl2;

Reference yield:

trans-1,4-Cyclohexanediyldimethylene bis(chloroformate) (46744-84-7) → C14H28N2O2(2+)*2BF4(1-) (86217-98-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 4 h / 3 - 6 °C

2: 55 percent / NaBF₄ / dimethylformamide / 2 h / Ambient temperature

With sodium tetrafluoroborate; In N,N-dimethyl-formamide;

DOI:10.1021/jo00163a047

Reference yield:

trans-1,4-Cyclohexanediyldimethylene bis(chloroformate) (46744-84-7) → trans-1,4-Bis(hydroxymethyl)cyclohexanediformate (86218-05-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 4 h / 3 - 6 °C

2: H₂O / dimethylformamide / Ambient temperature

With water; In N,N-dimethyl-formamide;

DOI:10.1021/jo00163a047

Downstream raw materials:

C₁₄H₂₈N₂O₂⁽²⁺⁾*2Cl^(1-)

C₁₄H₂₈N₂O₂⁽²⁺⁾*2BF₄^(1-)

trans-1,4-Bis-cyclohexane

trans-1,4-Bis(hydroxymethyl)cyclohexanediformate