C₃₂H₃₆N₂O₆

Base Information

Chemical Name:C₃₂H₃₆N₂O₆
CAS No.:1462886-62-9
Molecular Formula:C₃₂H₃₆N₂O₆
Molecular Weight:544.648
Hs Code.:

C<sub>32</sub>H<sub>36</sub>N<sub>2</sub>O<sub>6</sub>

Synonyms:

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Chemical Property of C₃₂H₃₆N₂O₆

Chemical Property:

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Technology Process of C₃₂H₃₆N₂O₆

There total 9 articles about C₃₂H₃₆N₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: methyl 5-(4-aminophenoxy)-2-nitrobenzoate

: 1462886-62-9
C₃₂H₃₆N₂O₆

Guidance literature:: Multi-step reaction with 7 steps

1: sodium hydrogencarbonate / tetrahydrofuran / 20 °C

2: palladium 10% on activated carbon; methanol / ethyl acetate / 20 °C

3: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 20 °C

4: pyridine; dmap / 60 °C

5: trifluoroacetic acid / dichloromethane / 20 °C

6: triethylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dimethyl sulfoxide / 20 °C

7: water; sodium hydroxide / 50 °C

With pyridine; methanol; dmap; palladium 10% on activated carbon; water; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; triethylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/jm401202a

Reference yield:

: 123-30-8
4-amino-phenol

: 1462886-62-9
C₃₂H₃₆N₂O₆

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate / dimethyl sulfoxide / 75 °C

2: sodium hydrogencarbonate / tetrahydrofuran / 20 °C

3: palladium 10% on activated carbon; methanol / ethyl acetate / 20 °C

4: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 20 °C

5: pyridine; dmap / 60 °C

6: trifluoroacetic acid / dichloromethane / 20 °C

7: triethylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dimethyl sulfoxide / 20 °C

8: water; sodium hydroxide / 50 °C

With pyridine; methanol; dmap; palladium 10% on activated carbon; water; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; triethylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/jm401202a

Reference yield:

: 51282-49-6
methyl 5-chloro-2-nitrobenzoate

: 1462886-62-9
C₃₂H₃₆N₂O₆

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate / dimethyl sulfoxide / 75 °C

2: sodium hydrogencarbonate / tetrahydrofuran / 20 °C

3: palladium 10% on activated carbon; methanol / ethyl acetate / 20 °C

4: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 20 °C

5: pyridine; dmap / 60 °C

6: trifluoroacetic acid / dichloromethane / 20 °C

7: triethylamine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate / dimethyl sulfoxide / 20 °C

8: water; sodium hydroxide / 50 °C

With pyridine; methanol; dmap; palladium 10% on activated carbon; water; sodium tris(acetoxy)borohydride; sodium hydrogencarbonate; potassium carbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; acetic acid; triethylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; ethyl acetate;
DOI:10.1021/jm401202a