(Z)-7-{(1R,2R,3R)-3-(tert-Butyl-dimethyl-silanyloxy)-2-[(E)-3-(4-methoxy-benzyloxy)-oct-1-enyl]-5-oxo-cyclopentyl}-hept-5-enoic acid methyl ester

Base Information

• Chemical Name: (Z)-7-{(1R,2R,3R)-3-(tert-Butyl-dimethyl-silanyloxy)-2-[(E)-3-(4-methoxy-benzyloxy)-oct-1-enyl]-5-oxo-cyclopentyl}-hept-5-enoic acid methyl ester
• CAS No.: 128683-95-4
• Molecular Formula: C₃₅H₅₆O₆Si
• Molecular Weight: 600.912

Synonyms:

Chemical Property of (Z)-7-{(1R,2R,3R)-3-(tert-Butyl-dimethyl-silanyloxy)-2-[(E)-3-(4-methoxy-benzyloxy)-oct-1-enyl]-5-oxo-cyclopentyl}-hept-5-enoic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of (Z)-7-{(1R,2R,3R)-3-(tert-Butyl-dimethyl-silanyloxy)-2-[(E)-3-(4-methoxy-benzyloxy)-oct-1-enyl]-5-oxo-cyclopentyl}-hept-5-enoic acid methyl ester

There total 4 articles about (Z)-7-{(1R,2R,3R)-3-(tert-Butyl-dimethyl-silanyloxy)-2-[(E)-3-(4-methoxy-benzyloxy)-oct-1-enyl]-5-oxo-cyclopentyl}-hept-5-enoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyldimethylsilyl vinyl ether (66031-93-4) → (Z)-7-{(1R,2R,3R)-3-(tert-Butyl-dimethyl-silanyloxy)-2-[(E)-3-(4-methoxy-benzyloxy)-oct-1-enyl]-5-oxo-cyclopentyl}-hept-5-enoic acid methyl ester (128683-95-4,128777-53-7)

Guidance literature:

Multi-step reaction with 3 steps

2: 85 percent / dibutyl ether / 2 h / 190 °C

In dibutyl ether;

Reference yield:

1-[1-((1E,3E)-4-Iodo-buta-1,3-dienyl)-hexyloxymethyl]-4-methoxy-benzene (128683-91-0) → (Z)-7-{(1R,2R,3R)-3-(tert-Butyl-dimethyl-silanyloxy)-2-[(E)-3-(4-methoxy-benzyloxy)-oct-1-enyl]-5-oxo-cyclopentyl}-hept-5-enoic acid methyl ester (128683-95-4,128777-53-7)

Guidance literature:

Multi-step reaction with 3 steps

2: 85 percent / dibutyl ether / 2 h / 190 °C

In dibutyl ether;

Reference yield:

Acetic acid (1R,2R)-2-(tert-butyl-dimethyl-silanyloxy)-1-[(1E,3E)-5-(4-methoxy-benzyloxy)-deca-1,3-dienyl]-cyclopropyl ester (128683-92-1,128777-50-4) → (Z)-7-{(1R,2R,3R)-3-(tert-Butyl-dimethyl-silanyloxy)-2-[(E)-3-(4-methoxy-benzyloxy)-oct-1-enyl]-5-oxo-cyclopentyl}-hept-5-enoic acid methyl ester (128683-95-4,128777-53-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / dibutyl ether / 2 h / 190 °C

In dibutyl ether;

upstream raw materials:

methyl (5Z)-7-iodo-5-heptenoate

Acetic acid (3R,4R)-4-(tert-butyl-dimethyl-silanyloxy)-3-[(E)-3-(4-methoxy-benzyloxy)-oct-1-enyl]-cyclopent-1-enyl ester

tert-butyldimethylsilyl vinyl ether

1-[1-((1E,3E)-4-Iodo-buta-1,3-dienyl)-hexyloxymethyl]-4-methoxy-benzene

Downstream raw materials:

(+/-)-prostaglandin E₂ methyl ester

(+/-)-15-epi-prostaglandin E₂ methyl ester

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