2-methylmercapto-4-phenyl-3,4,5,6-tetrahydrobenzoquinazoline hydroiodide

Base Information

• Chemical Name: 2-methylmercapto-4-phenyl-3,4,5,6-tetrahydrobenzoquinazoline hydroiodide
• CAS No.: 85660-19-1
• Molecular Formula: C₁₉H₁₈N₂S*HI
• Molecular Weight: 434.344

Synonyms:

Chemical Property of 2-methylmercapto-4-phenyl-3,4,5,6-tetrahydrobenzoquinazoline hydroiodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 2-methylmercapto-4-phenyl-3,4,5,6-tetrahydrobenzoquinazoline hydroiodide

There total 1 articles about 2-methylmercapto-4-phenyl-3,4,5,6-tetrahydrobenzoquinazoline hydroiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-benzylidene-1-tetralone (6261-32-1) → 2-methylmercapto-4-phenyl-3,4,5,6-tetrahydrobenzoquinazoline hydroiodide (85660-19-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent / NaOC₂H₅

2: 78 percent

With sodium ethanolate;

Reference yield: 82.0%

2-methylmercapto-4-phenyl-3,4,5,6-tetrahydrobenzoquinazoline hydroiodide (85660-19-1) → 2-Methylsulfanyl-4-phenyl-5,6-dihydro-benzo[h]quinazoline (85660-23-7)

Guidance literature:

With oxygen;

Reference yield:

2-methylmercapto-4-phenyl-3,4,5,6-tetrahydrobenzoquinazoline hydroiodide (85660-19-1) → 2-methylmercapto-4-phenyl-3,4,5,6-tetrahydrobenzoquinazoline (85660-21-5)

Guidance literature:

With potassium hydroxide; at 0 ℃;

upstream raw materials:

2-benzylidene-1-tetralone

Downstream raw materials:

2-methylmercapto-4-phenyl-3,4,5,6-tetrahydrobenzoquinazoline

2-Methylsulfanyl-4-phenyl-5,6-dihydro-benzo[h]quinazoline

2-methylmercapto-4-phenylbenzoquinazoline

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