1-phenylethylphosphonic dichloride

Base Information

Chemical Name:1-phenylethylphosphonic dichloride
CAS No.:20615-08-1
Molecular Formula:C₈H₉Cl₂OP
Molecular Weight:223.039
Hs Code.:

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Suppliers and Price of 1-phenylethylphosphonic dichloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenylethylphosphonic dichloride

Chemical Property:

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Technology Process of 1-phenylethylphosphonic dichloride

There total 3 articles about 1-phenylethylphosphonic dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 33973-48-7
diethyl (1-phenylethyl)phosphonate

: 20615-08-1
1-phenylethylphosphonic dichloride

Guidance literature:: Multi-step reaction with 2 steps

1: conc. HCl / 7 h / bath temperature 120 deg C

2: thionyl chloride / dimethylformamide / 3 h / bath temperature 90 deg C

With hydrogenchloride; thionyl chloride; In N,N-dimethyl-formamide;
DOI:10.1039/P19940003261

Reference yield:

: 585-71-7,38661-81-3
(1-bromoethyl)benzne

: 20615-08-1
1-phenylethylphosphonic dichloride

Guidance literature:: Multi-step reaction with 3 steps

1: 2 h / bath temperature 175 deg C

2: conc. HCl / 7 h / bath temperature 120 deg C

3: thionyl chloride / dimethylformamide / 3 h / bath temperature 90 deg C

With hydrogenchloride; thionyl chloride; In N,N-dimethyl-formamide;
DOI:10.1039/P19940003261