Li(THF)4 tetraisobutylaluminate

Base Information

Chemical Name:Li(THF)4 tetraisobutylaluminate
CAS No.:1004325-01-2
Molecular Formula:C₁₆H₃₂LiO₄*C₁₆H₃₆Al
Molecular Weight:550.812
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Li(THF)4 tetraisobutylaluminate

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Technology Process of Li(THF)4 tetraisobutylaluminate

There total 1 articles about Li(THF)4 tetraisobutylaluminate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 109-72-8,29786-93-4
n-butyllithium

: 20383-28-2
N,N-diisopropyl benzamide

: 100-99-2,130565-62-7
triisobutylaluminum

: 1004325-02-3
(THF)3Li(OCN(iPr)2(C₆H₄)triisobutylaluminate

: 1004325-01-2
Li(THF)4 tetraisobutylaluminate

Guidance literature:: With 2,2,6,6-tetramethylpiperidine; In tetrahydrofuran; hexane; (Ar), stoich., BuLi in hexane added to mixt. of THF and TMPH at -78°C, stirred at 0°C for 10 min, treated with Al complex in hexane at -78°C, stirred for 30 min at 0°C, treated with benzamide at -78°C, stirred at room; cooled, evapd.(vac.), treated with hexane, cooled to -27°C, elem.anal.;
DOI:10.1039/b713913f