Technology Process of 2-benzylidene-3-oxo-5-phenyl-2,3-dihydrotellurophene
There total 3 articles about 2-benzylidene-3-oxo-5-phenyl-2,3-dihydrotellurophene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride; 1,3-di-tert-butyl-1,1,3,3-tetramethyldisilatellurane;
In
tert-butyl alcohol;
for 1h;
Ambient temperature;
DOI:10.1021/jo00349a030
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 72 percent / Na2Cr2O7 in aq. H2SO4 / acetone
2: 28 percent / bis((tert-butyldimethylsilyl) telluride, tetra-n-butylammonium fluoride / 2-methyl-propan-2-ol / 1 h / Ambient temperature
With
sodium dichromate; sulfuric acid; tetrabutyl ammonium fluoride; 1,3-di-tert-butyl-1,1,3,3-tetramethyldisilatellurane;
In
acetone; tert-butyl alcohol;
DOI:10.1021/jo00349a030
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) EtBr, Mg, I2 / 1.) ether, RT, 3 h
2: 72 percent / Na2Cr2O7 in aq. H2SO4 / acetone
3: 28 percent / bis((tert-butyldimethylsilyl) telluride, tetra-n-butylammonium fluoride / 2-methyl-propan-2-ol / 1 h / Ambient temperature
With
sodium dichromate; sulfuric acid; tetrabutyl ammonium fluoride; iodine; ethidium Bromide; 1,3-di-tert-butyl-1,1,3,3-tetramethyldisilatellurane; magnesium;
In
acetone; tert-butyl alcohol;
DOI:10.1021/jo00349a030
